Technology Process of Ethanol, 2-[2-[(acetyloxy)methoxy]ethoxy]-, benzoate
There total 4 articles about Ethanol, 2-[2-[(acetyloxy)methoxy]ethoxy]-, benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1002/ejoc.201800380
- Guidance literature:
-
With
silver(I) acetate;
In
acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: mercury(II) diacetate / tetrahydrofuran; water / 0.25 h / Inert atmosphere
1.2: Inert atmosphere
1.3: 0.33 h / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2.2: 20 - 90 °C / Inert atmosphere
3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 3-chloro-benzenecarboperoxoic acid; tetrabutylammomium bromide / dichloromethane / 6 h / 20 °C / Inert atmosphere
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; mercury(II) diacetate; tetrabutylammomium bromide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201800380
