2-(Acetyloxy)propanoic acid 5-methyl-2-isopropylcyclohexyl ester

Base Information

• Chemical Name: 2-(Acetyloxy)propanoic acid 5-methyl-2-isopropylcyclohexyl ester
• CAS No.: 64870-66-2
• Molecular Formula: C₁₅H₂₆O₄
• Molecular Weight: 270.369
• Mol file: 64870-66-2.mol

Synonyms:

Chemical Property of 2-(Acetyloxy)propanoic acid 5-methyl-2-isopropylcyclohexyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(Acetyloxy)propanoic acid 5-methyl-2-isopropylcyclohexyl ester

There total 13 articles about 2-(Acetyloxy)propanoic acid 5-methyl-2-isopropylcyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

piperitone (89-81-6,6091-52-7) → (S)-2-Acetoxy-propionic acid (1S,2R,5R)-2-isopropyl-5-methyl-cyclohexyl ester (64870-66-2)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄

3: H₂ / 10 percent Pd/C / diethyl ether; diethyl ether / 1 h

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; 1: Reduction / 2: Acylation / 3: Catalytic hydrogenation;

DOI:10.1007/BF02040199

Reference yield:

piperitone (89-81-6,6091-52-7) → (S)-2-Acetoxy-propionic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester (64870-66-2)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄

3: H₂ / 10 percent Pd/C / diethyl ether; diethyl ether / 1 h

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; 1: Reduction / 2: Acylation / 3: Catalytic hydrogenation;

DOI:10.1007/BF02040199

Reference yield:

piperitone (89-81-6,6091-52-7) → (S)-2-Acetoxy-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (64870-66-2)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄

3: H₂ / 10 percent Pd/C / diethyl ether; diethyl ether / 1 h

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; 1: Reduction / 2: Acylation / 3: Catalytic hydrogenation;

DOI:10.1007/BF02040199

upstream raw materials:

piperitone

trans-6-isopropyl-3-methylcyclohex-2-en-1-ol

(S)-menthyl lactate

acetic anhydride

Refernces

• 1、 Wimalaratne,Slessor,Borden,Chong,Abate. "Isolation and identification of house fly, Musca domestica L., repellents from pepper tree, Schinus molle L.". . p. 49 - 59. Retrieved 2007/10/03.