Osmium, (carbonothioyl)carbonyltris(triphenylphosphine)-

Base Information

Chemical Name:Osmium, (carbonothioyl)carbonyltris(triphenylphosphine)-
CAS No.:64883-46-1
Molecular Formula:C₅₆H₄₅OOsP₃S
Molecular Weight:1049.16
Hs Code.:

Synonyms:

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Chemical Property of Osmium, (carbonothioyl)carbonyltris(triphenylphosphine)-

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Technology Process of Osmium, (carbonothioyl)carbonyltris(triphenylphosphine)-

There total 1 articles about Osmium, (carbonothioyl)carbonyltris(triphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 64883-48-3
OsH₂(CS)(P(C₆H₅)3)3

: 82468-43-7,64883-46-1
osmium(carbonyl)(CS)(triphenylphosphine)3

Guidance literature:: With sodium hydroxide; triphenylphosphine; In methanol; dichloromethane; byproducts: H2, HClO4; to a soln. of Os-complex in CH2Cl2-MeOH aq. HClO4 was added, stirred for 2 h under an atm. of CO, CH2Cl2 was removed, MeOH and PPh3 were added,N2 was passed for 10 min, heated under reflux, NaOH was added, cooled to room temp.; further reagents; collected, washed with MeOH and hexane, dried at room temp.; elem. anal.;
DOI:10.1016/S0022-328X(00)81955-5

Reference yield: 97.3%

: 82468-43-7,64883-46-1
osmium(carbonyl)(CS)(triphenylphosphine)3

: 65105-17-1
Os(CS₂)(CO)(CS)(P(C₆H₅)3)2

Guidance literature:: With carbon disulfide; In benzene; Os-complex was heated under reflux in C6H6 containing CS2 for 30 min; evapd., EtOH was added, C6H6 was removed, collected, washed with EtOH; elem. anal.;
DOI:10.1016/S0022-328X(00)81955-5

Reference yield: 87.5%

: 82468-43-7,64883-46-1
osmium(carbonyl)(CS)(triphenylphosphine)3

: 61926-59-8
Os(CO)2(CS)(P(C₆H₅)3)2

Guidance literature:: With carbon monoxide; In benzene; a soln. of Os-complex in C6H6 was heated under CO (100 psi) to 160°C, EtOH was added; evapd., collected, washed with EtOH hexane, recrystd. from CH2Cl2-EtOH; elem. anal.;
DOI:10.1016/S0022-328X(00)81955-5