Hydrouracil, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-5-methyl-, (5S)-

Base Information

• Chemical Name: Hydrouracil, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-5-methyl-, (5S)-
• CAS No.: 19140-39-7

Synonyms:

Chemical Property of Hydrouracil, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-5-methyl-, (5S)-

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydrouracil, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-5-methyl-, (5S)-

There total 4 articles about Hydrouracil, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-5-methyl-, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4) → (5S)-1-(2-deoxy-β-D-erythro-pentofuranosyl)-5,6-dihydrothymine (19140-39-7) + (+)-(5R)-5,6-dihydrothymidine (78216-59-8) + (5R,5'S)-bi-5,6-dihydrothymidine (87517-85-9)

Guidance literature:

With water; sodium formate; Ambient temperature; Irradiation; pH 7.0;

DOI:10.1021/ja00360a047

Reference yield: 29.0%

→ (5S)-1-(2-deoxy-β-D-erythro-pentofuranosyl)-5,6-dihydrothymine (19140-39-7) + (+)-(5R)-5,6-dihydrothymidine (78216-59-8) + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4)

Guidance literature:

With water; sodium formate; Ambient temperature; Irradiation; pH 7.0;

DOI:10.1021/ja00360a047

Reference yield: 9.8%

thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4) → (5S)-1-(2-deoxy-β-D-erythro-pentofuranosyl)-5,6-dihydrothymine (19140-39-7) + cis-syn thymidine<>thymidine (33407-74-8) + trans-anti thymidine<>thymidine + (+) cis-anti thymidine<>thymidine

Guidance literature:

In water; acetone; for 18h; Further byproducts given; Irradiation;

upstream raw materials:

thymidine

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