D-Homotestosterone

Base Information

Chemical Name:D-Homotestosterone
CAS No.:3818-24-4
Molecular Formula:C20H30O2
Molecular Weight:302.451
Hs Code.:
UNII:1X7AW8BV0P
Nikkaji Number:J2.793.864G
Wikidata:Q27148957
Mol file:3818-24-4.mol

Synonyms:D-Homotestosterone;Homotestosterone, D-;3818-24-4;1X7AW8BV0P;NSC-58850;17abeta-Hydroxy-D-homoandrost-4-en-3-one;(4aR,4bS,6aS,7S,10aS,10bR)-7-hydroxy-4a,6a-dimethyl-4,4b,5,6,7,8,9,10,10a,10b,11,12-dodecahydro-3H-chrysen-2-one;2(3H)-Chrysenone, 4,4a,4b,5,6,6a,7,8,9,10,10a,10b,11,12-tetradecahydro-7-hydroxy-4a,6a-dimethyl-, (4aR,4bS,6aS,7S,10aS,10bR)-;UNII-1X7AW8BV0P;SCHEMBL26570105;CHEBI:79820;Q27148957;D-Homoandrost-4-en-3-one, 17a-hydroxy-, (17abeta)-;D-HOMOANDROST-4-EN-3-ONE, 17A-HYDROXY-, (17A.BETA.)-;2(3H)-CHRYSENONE, 4,4A,4B,5,6,6A,7,8,9,10,10A,10B,11,12-TETRADECAHYDRO-7-HYDROXY-4A,6A-DIMETHYL-, (4AR-(4A.ALPHA.,4B.BETA.,6A.ALPHA.,7.ALPHA.,10A.BETA.,10B.ALPHA.))-;2(3H)-Chrysenone, 4,4a,4b,5,6,6a,7,8,9,10,10a,10b,11,12-tetradecahydro-7-hydroxy-4a,6a-dimethyl-, (4ar-(4aalpha,4bbeta,6aalpha,7alpha,10abeta,10balpha))-

Suppliers and Price of D-Homotestosterone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of D-Homotestosterone

Chemical Property:

Vapor Pressure:7.19E-10mmHg at 25°C
Boiling Point:447°Cat760mmHg
Flash Point:190.5°C
Density:1.1g/cm³
XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:302.224580195
Heavy Atom Count:22
Complexity:522

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC12CCC3C(C1CCCC2O)CCC4=CC(=O)CCC34C
Isomeric SMILES:C[C@]12CC[C@H]3[C@H]([C@@H]1CCC[C@@H]2O)CCC4=CC(=O)CC[C@]34C

Technology Process of D-Homotestosterone

There total 16 articles about D-Homotestosterone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5978-08-5
1-chloro-4-(1,3-dioxolane)-n-pentane

: 3818-24-4,17553-96-7
(+/-)-Homotestosterone

Guidance literature:: Multi-step reaction with 5 steps

1: 6.9 g / tetrahydrofuran / 1.) -5 deg C, 0.5 h, 2.) reflux, 15 min

2: CrO₃, H₂SO₄ / acetone / -20 °C

3: 1.) Li, t-BuOH, 3.) 4percent aq. KOH / 1.) NH₃ (l), ether, 0.75 h, 2.) ether, -78 deg C to -20 deg C, 1.5 h, 3.) MeOH, reflux, 3 h

4: 1.) Li / 1.) liquid NH₃, -33 deg C, 1.5 h, 2.) NH₃ (liquid), ether, -33 deg C, 3 h

5: 1.) 10percent aq. HCl, 2.) 4percent aq. KOH / 1.) acetone, 18 h, r.t., 2.) MeOH, reflux, 3 h

With chromium(VI) oxide; hydrogenchloride; potassium hydroxide; sulfuric acid; lithium; tert-butyl alcohol; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)88591-4

Reference yield:

: 86680-10-6
6-(2-Methyl-[1,3]dioxolan-2-yl)-2-trimethylsilanyl-hex-1-en-3-ol

: 3818-24-4,17553-96-7
(+/-)-Homotestosterone

Guidance literature:: Multi-step reaction with 4 steps

1: CrO₃, H₂SO₄ / acetone / -20 °C

2: 1.) Li, t-BuOH, 3.) 4percent aq. KOH / 1.) NH₃ (l), ether, 0.75 h, 2.) ether, -78 deg C to -20 deg C, 1.5 h, 3.) MeOH, reflux, 3 h

3: 1.) Li / 1.) liquid NH₃, -33 deg C, 1.5 h, 2.) NH₃ (liquid), ether, -33 deg C, 3 h

4: 1.) 10percent aq. HCl, 2.) 4percent aq. KOH / 1.) acetone, 18 h, r.t., 2.) MeOH, reflux, 3 h

With chromium(VI) oxide; hydrogenchloride; potassium hydroxide; sulfuric acid; lithium; tert-butyl alcohol; In acetone;
DOI:10.1016/S0040-4020(01)88591-4