Benzenemethanol, 4-iodo-, hydrogen phosphate

Base Information

• Chemical Name: Benzenemethanol, 4-iodo-, hydrogen phosphate
• CAS No.: 64976-63-2
• Molecular Formula: C₁₄H₁₃I₂O₄P
• Molecular Weight: 530.038
• Mol file: 64976-63-2.mol

Synonyms:

Chemical Property of Benzenemethanol, 4-iodo-, hydrogen phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, 4-iodo-, hydrogen phosphate

There total 1 articles about Benzenemethanol, 4-iodo-, hydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosphoric acid tris-(4-iodo-benzyl ester) (60599-65-7) → 1-iodo-4-(iodomethyl)benzene (287208-66-6) + phosphoric acid bis-(4-iodo-benzyl ester) (64976-63-2)

Guidance literature:

With butanone; sodium iodide;

DOI:10.1021/ja01625a045

Reference yield:

phosphoric acid bis-(4-iodo-benzyl ester) (64976-63-2) → chlorophosphoric acid bis-(4-iodo-benzyl ester) (856802-10-3)

Guidance literature:

With chloroform; phosphorus pentachloride;

DOI:10.1021/ja01625a045

Reference yield:

phosphoric acid bis-(4-iodo-benzyl ester) (64976-63-2) → phosphoric acid butyl ester-(4-iodo-benzyl ester)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃; PCl₅

2: butan-1-ol; pyridine; CHCl₃ / Erwaermen des Reaktionsprodukts mit NaI in Aceton

With pyridine; chloroform; phosphorus pentachloride; butan-1-ol;

DOI:10.1021/ja01625a045

upstream raw materials:

phosphoric acid tris-(4-iodo-benzyl ester)

Downstream raw materials:

diphosphoric acid tetrakis-(4-iodo-benzyl ester)

chlorophosphoric acid bis-(4-iodo-benzyl ester)