Benzenemethanol, a-[(2,6-dimethoxyphenoxy)methyl]-4-hydroxy-3,5-dimethoxy-

Base Information

Chemical Name:Benzenemethanol, a-[(2,6-dimethoxyphenoxy)methyl]-4-hydroxy-3,5-dimethoxy-
CAS No.:65109-39-9
Molecular Formula:C18H22O7
Molecular Weight:350.368
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanol, a-[(2,6-dimethoxyphenoxy)methyl]-4-hydroxy-3,5-dimethoxy-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, a-[(2,6-dimethoxyphenoxy)methyl]-4-hydroxy-3,5-dimethoxy-

There total 10 articles about Benzenemethanol, a-[(2,6-dimethoxyphenoxy)methyl]-4-hydroxy-3,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 174421-46-6
2-(2,6-dimethoxyphenoxy)-1-(3,4,5-trimethoxyphenyl)ethanone

: 65109-39-9
4-(2-(2,6-dimethoxyphenoxy)-1-hydroxyethyl)-2,6-dimethoxyphenol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃;
DOI:10.1021/ol401065r

Reference yield:

: 41628-47-1
ethyl (2E)-3-[4-hydroxy-3,5-bis(methyloxy)phenyl]-2-propenoate

: 65109-39-9
4-(2-(2,6-dimethoxyphenoxy)-1-hydroxyethyl)-2,6-dimethoxyphenol

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / toluene / 4 h / Cooling with ice

2: horseradish peroxidase; dihydrogen peroxide; sodium dihydrogenphosphate / acetone; water / 2.83 h

3: sodium hydroxide / 1 h / 170 °C

4: potassium carbonate / acetone; N,N-dimethyl-formamide / 50 °C

5: hydrogen; palladium 10% on activated carbon / ethanol

With sodium dihydrogenphosphate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; diisobutylaluminium hydride; potassium carbonate; sodium hydroxide; horseradish peroxidase; In ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1039/d0gc01658f

Reference yield:

: 20675-96-1
trans-sinapyl alcohol

: 65109-39-9
4-(2-(2,6-dimethoxyphenoxy)-1-hydroxyethyl)-2,6-dimethoxyphenol

Guidance literature:: Multi-step reaction with 4 steps

1: horseradish peroxidase; dihydrogen peroxide; sodium dihydrogenphosphate / acetone; water / 2.83 h

2: sodium hydroxide / 1 h / 170 °C

3: potassium carbonate / acetone; N,N-dimethyl-formamide / 50 °C

4: hydrogen; palladium 10% on activated carbon / ethanol

With sodium dihydrogenphosphate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; sodium hydroxide; horseradish peroxidase; In ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/d0gc01658f