1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine]

Base Information

Chemical Name:1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine]
CAS No.:65113-31-7
Molecular Formula:C₂₄H₂₆Cl₂P₂
Molecular Weight:447.324
Hs Code.:
DSSTox Substance ID:DTXSID401180837

Synonyms:DTXSID401180837;1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine];65113-31-7

Suppliers and Price of 1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine]

Chemical Property:

XLogP3:6.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:10
Exact Mass:446.0886802
Heavy Atom Count:28
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(CCCCl)C2=CC=CC=C2P(CCCCl)C3=CC=CC=C3

Technology Process of 1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine]

There total 1 articles about 1,1'-(1,2-Phenylene)bis[1-(3-chloropropyl)-1-phenylphosphine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65113-31-7
1,2-Bis-[(3-chloro-propyl)-phenyl-phosphanyl]-benzene

Guidance literature:: 3, Br-(CH2)3-Cl;
DOI:10.1021/ja00466a049

Reference yield:

: 65113-31-7
o-bis((3-chloropropyl)phenylphosphino)benzene

: 65113-30-6,78339-67-0,78339-68-1
cis,trans,cis-2,6,13,17-tetraphenyl-2,6-13,17-tetraphosphatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1) THF, hexane, -78 deg C; 2) THF, 24 h

2: 0.5 h / 185 °C

With n-butyllithium;
DOI:10.1021/ja00403a041

Reference yield:

: 38023-29-9
1,2-diphenylphosphinobenzene

: 65113-31-7
o-bis((3-chloropropyl)phenylphosphino)benzene

: 65113-30-6,78339-67-0,78339-68-1
cis,trans,cis-2,6,13,17-tetraphenyl-2,6-13,17-tetraphosphatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexane

: 65113-30-6,78339-67-0,78339-68-1
cis,cis,cis-2,6,13,17-tetraphenyl-2,6-13,17-tetraphosphatricyclo<16.4.0.0^7,12>docosa-7(12),8,10,1(18),19,21-hexane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1) THF, hexane, -78 deg C; 2) THF, 24 h;
DOI:10.1021/ja00403a041