Benzenepropanamine, N-hydroxy-a-methyl-

Base Information

• Chemical Name: Benzenepropanamine, N-hydroxy-a-methyl-
• CAS No.: 65266-76-4
• Molecular Formula: C10H15NO
• Molecular Weight: 165.235

Synonyms:Benzenepropanamine, N-hydroxy-a-methyl-

Chemical Property of Benzenepropanamine, N-hydroxy-a-methyl-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of Benzenepropanamine, N-hydroxy-a-methyl-

There total 2 articles about Benzenepropanamine, N-hydroxy-a-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-phenyl-2-butanone oxime (66417-92-3,104260-82-4,6944-54-3) → N-(1-Methyl-3-phenyl-propyl)-hydroxylamine (65266-76-4)

Guidance literature:

With borane pyridine complex; In ethanol; Product distribution; reduction of oxime derivatives;

DOI:10.1248/cpb.29.1615

Reference yield:

→ N-(1-Methyl-3-phenyl-propyl)-hydroxylamine (65266-76-4)

Guidance literature:

Oxim 1c, Red. mit Pyridin-boran in Ggw. von Saeure;

DOI:10.1246/cl.1977.1279

Reference yield: 61.0%

N-(1-Methyl-3-phenyl-propyl)-hydroxylamine (65266-76-4) → 1,2,3,4-tetrahydro-2-methylquinoline (1780-19-4)

Guidance literature:

With trifluoroacetic acid; for 15h; Heating;

DOI:10.1248/cpb.29.1615

upstream raw materials:

4-phenyl-2-butanone oxime

Downstream raw materials:

1,2,3,4-tetrahydro-2-methylquinoline

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