Technology Process of ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate
There total 4 articles about ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
for 8h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 88 percent / CH2Cl2 / 0.75 h
2: 79 percent / 99 percent hydrazine hydrate / 10 percent Pd/C / methanol / 0.08 h / Heating
3: 76 percent / sodium nitrite, 1 N HCl / H2O; methanol / 2 h
4: 50 percent / Et3N / tetrahydrofuran / 8 h / Heating
With
hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 79 percent / 99 percent hydrazine hydrate / 10 percent Pd/C / methanol / 0.08 h / Heating
2: 76 percent / sodium nitrite, 1 N HCl / H2O; methanol / 2 h
3: 50 percent / Et3N / tetrahydrofuran / 8 h / Heating
With
hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; water;