ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate

Base Information

Chemical Name:ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate
CAS No.:146495-61-6
Molecular Formula:C₁₅H₁₆N₆O₃
Molecular Weight:328.33
Hs Code.:
Mol file:146495-61-6.mol

Synonyms:Pyrazolo[3,4-d]-1,2,3-triazole,glycine deriv.

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Chemical Property of ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate

Chemical Property:

Density:1.43g/cm³

Purity/Quality:

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Technology Process of ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate

There total 4 articles about ethyl N-[(6-methyl-4-phenylpyrazolo[3,4-d][1,2,3]triazol-3(4H)-yl)carbonyl]glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 220830-44-4
C₁₅H₁₆N₆O₃

: 146495-61-6
[(6-Methyl-4-phenyl-4H-pyrazolo[3,4-d][1,2,3]triazole-3-carbonyl)-amino]-acetic acid ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 8h; Heating;

Reference yield:

: 58663-02-8
5-phenyl-7-methylpyrazolo<4,3-c><1,2,5>oxadiazin-3(5H)-one

: 146495-61-6
[(6-Methyl-4-phenyl-4H-pyrazolo[3,4-d][1,2,3]triazole-3-carbonyl)-amino]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / CH₂Cl₂ / 0.75 h

2: 79 percent / 99 percent hydrazine hydrate / 10 percent Pd/C / methanol / 0.08 h / Heating

3: 76 percent / sodium nitrite, 1 N HCl / H₂O; methanol / 2 h

4: 50 percent / Et₃N / tetrahydrofuran / 8 h / Heating

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 146495-46-7
[3-(5-Methyl-4-nitroso-2-phenyl-2H-pyrazol-3-yl)-ureido]-acetic acid ethyl ester

: 146495-61-6
[(6-Methyl-4-phenyl-4H-pyrazolo[3,4-d][1,2,3]triazole-3-carbonyl)-amino]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / 99 percent hydrazine hydrate / 10 percent Pd/C / methanol / 0.08 h / Heating

2: 76 percent / sodium nitrite, 1 N HCl / H₂O; methanol / 2 h

3: 50 percent / Et₃N / tetrahydrofuran / 8 h / Heating

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol; water;