3-Methyl-2,5-dinitroaniline

Base Information

Chemical Name:3-Methyl-2,5-dinitroaniline
CAS No.:65321-68-8
Molecular Formula:C7H7N3O4
Molecular Weight:197.15
Hs Code.:
DSSTox Substance ID:DTXSID70500360
Nikkaji Number:J1.449.124D
Wikidata:Q82351892

Synonyms:3-Methyl-2,5-dinitroaniline;3-amino-2,5-dinitrotoluene;65321-68-8;SCHEMBL11043450;DTXSID70500360;QGYMOSRHASJNGZ-UHFFFAOYSA-N

Suppliers and Price of 3-Methyl-2,5-dinitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Methyl-2,5-dinitroaniline

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:197.04365571
Heavy Atom Count:14
Complexity:246

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1[N+](=O)[O-])N)[N+](=O)[O-]

Technology Process of 3-Methyl-2,5-dinitroaniline

There total 4 articles about 3-Methyl-2,5-dinitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70343-15-6
2,5-dinitro-3-methylbenzoic acid

: 65321-68-8
2,5-dinitro-3-methylaniline

Guidance literature:: With sodium azide; sulfuric acid; sulfur trioxide;
DOI:10.1021/jo01328a037

Reference yield:

: 70343-13-4
7-methyl-5-nitro-1H-indole-2,3-dione

: 65321-68-8
2,5-dinitro-3-methylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: (i) NaOH, (ii) H₂O₂, (iii) AcOH

2: (CF₃CO)2O, CF₃CO₂H, H₂O₂

3: NaN₃, SO₃/H₂SO₄

With sodium azide; sulfuric acid; sulfur trioxide; dihydrogen peroxide; trifluoroacetic acid; trifluoroacetic anhydride;
DOI:10.1021/jo01328a037

Reference yield:

: 70343-14-5
2-amino-3-methyl-5-nitrobenzoic acid

: 65321-68-8
2,5-dinitro-3-methylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: (CF₃CO)2O, CF₃CO₂H, H₂O₂

2: NaN₃, SO₃/H₂SO₄

With sodium azide; sulfuric acid; sulfur trioxide; dihydrogen peroxide; trifluoroacetic acid; trifluoroacetic anhydride;
DOI:10.1021/jo01328a037