10-Octadecenoic acid, 9-hydroxy-12-oxo-, methyl ester, (E)-

Base Information

Chemical Name:10-Octadecenoic acid, 9-hydroxy-12-oxo-, methyl ester, (E)-
CAS No.:65372-03-4
Molecular Formula:C₁₉H₃₄O₄
Molecular Weight:326.477
Hs Code.:

Synonyms:

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Chemical Property of 10-Octadecenoic acid, 9-hydroxy-12-oxo-, methyl ester, (E)-

Chemical Property:

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Technology Process of 10-Octadecenoic acid, 9-hydroxy-12-oxo-, methyl ester, (E)-

There total 1 articles about 10-Octadecenoic acid, 9-hydroxy-12-oxo-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34724-40-8
methyl 12-oxo-9,10-epoxyoctadecanoate

: 10038-16-1
methyl 8-(5-hexyl-2-furyl)-octanoate

: 65372-08-9
9.12-Dioxooctadecansaeure-methylester

: 65372-03-4
methyl 9-hydroxy-12-oxooctadec-10(E)-enoate

Guidance literature:: With aluminum oxide; In dichloromethane;

Reference yield:

: 65372-03-4
methyl 9-hydroxy-12-oxooctadec-10(E)-enoate

: 122221-62-9
2-(6'-methoxycarbonylhexyl)-3-phenylethenylcyclopent-2-enone

Guidance literature:: Multi-step reaction with 8 steps

1: 7.3 g / pyridine / 9 h / Ambient temperature

2: 90 percent / BF₃*OEt₂ / benzene / Ambient temperature

3: 2 g / H₂ / ethanol / 0.5 h / 760 Torr / Ambient temperature

4: 1) BuLi / 1) THF, petrol ether, -45 deg C, 30 min, 2a) -45 deg C, 1 h, 2b) up to 0 deg C

5: 80 percent / K₂CO₃ / methanol / 2.5 h / Ambient temperature

6: 2.9 g / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h / Ambient temperature

7: 40 percent / aq.KOH / dioxane / 5.5 h / 52 - 57 °C

8: 72 mg / H₂, chinoline / 5percent Pd-BaSO₄ / ethanol / Ambient temperature

With pyridine; quinoline; potassium hydroxide; n-butyllithium; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; pyridinium chlorochromate; palladium on barium sulfate; In 1,4-dioxane; methanol; ethanol; dichloromethane; benzene;

Reference yield:

: 65372-03-4
methyl 9-hydroxy-12-oxooctadec-10(E)-enoate

: 122221-60-7
methyl 9,12-dioxo-14-phenyltetradec-13-yn-oate

Guidance literature:: Multi-step reaction with 6 steps

1: 7.3 g / pyridine / 9 h / Ambient temperature

2: 90 percent / BF₃*OEt₂ / benzene / Ambient temperature

3: 2 g / H₂ / ethanol / 0.5 h / 760 Torr / Ambient temperature

4: 1) BuLi / 1) THF, petrol ether, -45 deg C, 30 min, 2a) -45 deg C, 1 h, 2b) up to 0 deg C

5: 80 percent / K₂CO₃ / methanol / 2.5 h / Ambient temperature

6: 2.9 g / pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; n-butyllithium; boron trifluoride diethyl etherate; hydrogen; potassium carbonate; pyridinium chlorochromate; In methanol; ethanol; dichloromethane; benzene;