2,4-Pentadienamide, N,N-dimethyl-5-phenyl-, (Z,E)-

Base Information

Chemical Name:2,4-Pentadienamide, N,N-dimethyl-5-phenyl-, (Z,E)-
CAS No.:65378-68-9
Molecular Formula:C13H15NO
Molecular Weight:201.268
Hs Code.:

Synonyms:

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Chemical Property of 2,4-Pentadienamide, N,N-dimethyl-5-phenyl-, (Z,E)-

Chemical Property:

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Technology Process of 2,4-Pentadienamide, N,N-dimethyl-5-phenyl-, (Z,E)-

There total 6 articles about 2,4-Pentadienamide, N,N-dimethyl-5-phenyl-, (Z,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₁₃H₁₃NO

: 65378-68-9
(2Z,4E)-N,N-dimethyl-5-phenyl-2,4-pentadienamide

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; diethoxymethylane; lithium methanolate; copper dichloride; In tetrahydrofuran; at 20 ℃; for 8h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/d0ob02037k

Reference yield:

: 2680-03-7,68761-83-1
N,N-Dimethylacrylamide

: 140-10-3
(E)-3-phenylacrylic acid

: 65378-68-9
(2Z,4E)-N,N-dimethyl-5-phenyl-2,4-pentadienamide

: 21497-23-4
(2E,4E)-N,N-dimethyl-5-phenylpenta-2,4-dienamide

Guidance literature:: With palladium(II) trifluoroacetate; 2,2-dimethylpropanoic anhydride; bis[2-(diphenylphosphino)phenyl] ether; sodium chloride; In tetrahydrofuran; at 150 ℃; for 10h; Overall yield = 70 percent; Overall yield = 28.1 mg; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02462

Reference yield:

: 80220-97-9
(E)-3-(β-styryl)propiolic acid

: 65378-68-9
(2Z,4E)-N,N-dimethyl-5-phenyl-2,4-pentadienamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: copper dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; diethoxymethylane; lithium methanolate / tetrahydrofuran / 8 h / 20 °C / Inert atmosphere; Schlenk technique

With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; diethoxymethylane; lithium methanolate; dicyclohexyl-carbodiimide; copper dichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/d0ob02037k