Technology Process of 4-Quinolinecarboxylic acid, 3-methyl-2-phenyl-, methyl ester, 1-oxide
There total 7 articles about 4-Quinolinecarboxylic acid, 3-methyl-2-phenyl-, methyl ester, 1-oxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
acetic acid;
at 90 - 95 ℃;
for 7h;
Yield given;
DOI:10.1248/cpb.28.1157
- Guidance literature:
-
Multi-step reaction with 5 steps
1: NaOMe / methanol / 2 h / Heating
2: 35percent H2O2 / acetic acid / 7 h / 90 - 95 °C
3: CDCl3 / Irradiation
4: 11.3 percent / acetone; H2O / Ambient temperature
5: 35percent H2O2 / acetic acid / 7 h / 90 - 95 °C
With
dihydrogen peroxide; sodium methylate;
In
methanol; chloroform-d1; water; acetic acid; acetone;
DOI:10.1248/cpb.28.1157
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 33percent aq. KOH / ethanol / Heating
2: NaOMe / methanol / 2 h / Heating
3: 35percent H2O2 / acetic acid / 7 h / 90 - 95 °C
4: CDCl3 / Irradiation
5: 11.3 percent / acetone; H2O / Ambient temperature
6: 35percent H2O2 / acetic acid / 7 h / 90 - 95 °C
With
potassium hydroxide; dihydrogen peroxide; sodium methylate;
In
methanol; chloroform-d1; ethanol; water; acetic acid; acetone;
DOI:10.1248/cpb.28.1157
