1,1'-Methylenebis[4-azidobenzene]

Base Information

Chemical Name:1,1'-Methylenebis[4-azidobenzene]
CAS No.:2915-44-8
Molecular Formula:C13H10 N6
Molecular Weight:250.263
Hs Code.:2929909090
European Community (EC) Number:220-833-5
DSSTox Substance ID:DTXSID30951753
Nikkaji Number:J306.839K
Wikidata:Q82930174
Mol file:2915-44-8.mol

Synonyms:4,4'-Diazidodiphenylmethane;1,1'-METHYLENEBIS[4-AZIDOBENZENE];2915-44-8;1,1'-Methylenebis(4-azidobenzene);EINECS 220-833-5;Benzene, 1,1'-methylenebis(4-azido-;Benzene, 1,1'-methylenebis[4-azido-;Bis(4-azidophenyl)methane;4,4'-Bisazido-diphenylmethan;4,4'-Bisazido-diphenylmethane;SCHEMBL15590856;DTXSID30951753

Suppliers and Price of 1,1'-Methylenebis[4-azidobenzene]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,1'-Methylenebis[4-azidobenzene]

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：99.50000
Density:g/cm³
LogP:4.06652
XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:250.09669434
Heavy Atom Count:19
Complexity:331

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CC2=CC=C(C=C2)N=[N+]=[N-])N=[N+]=[N-]

Technology Process of 1,1'-Methylenebis[4-azidobenzene]

There total 2 articles about 1,1'-Methylenebis[4-azidobenzene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 101-77-9
4,4'-diamino diphenyl methane

: 2915-44-8
4,4'-diazidodiphenylmethane

Guidance literature:: 4,4'-diamino diphenyl methane; With toluene-4-sulfonic acid; sodium nitrite; In water; at 20 ℃; for 0.666667h;

With sodium azide; In water; at 20 ℃; Reagent/catalyst;
DOI:10.1055/s-0033-1339648

Reference yield:

: 2915-44-8
4,4'-diazidodiphenylmethane

Guidance literature:: 4,4'-Diaminodiphenylmethan, 1) NaNO2, 2) NaN3;

Reference yield: 90.0%

: 2915-44-8
4,4'-diazidodiphenylmethane

: 54060-30-9
3-acetylenephenylamine

: 1393716-45-4
3,3'-(1,1'-(4,4'-methylenebis(4,1-phenylene))bis(1,2,3-triazole-4,1-diyl))diamine

Guidance literature:: 4,4'-diazidodiphenylmethane; 3-acetylenephenylamine; In N,N-dimethyl-formamide; at 20 ℃;

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; for 24h;
DOI:10.5012/bkcs.2012.33.7.2193