Pyridine, 2-(1-(2-fluorophenyl)ethenyl-

Base Information

• Chemical Name: Pyridine, 2-(1-(2-fluorophenyl)ethenyl-
• CAS No.: 74309-53-8
• Molecular Formula: C13H10FN
• Molecular Weight: 199.2236
• DSSTox Substance ID: DTXSID20225319
• Wikidata: Q83104261

Synonyms:Pyridine, 2-(1-(2-fluorophenyl)ethenyl-;Pyridine, 2-[1-(2-fluorophenyl)ethenyl-;74309-53-8;DTXSID20225319

Chemical Property of Pyridine, 2-(1-(2-fluorophenyl)ethenyl-

Chemical Property:

• Vapor Pressure: 0.00401mmHg at 25°C
• Boiling Point: 288.6°Cat760mmHg
• Flash Point: 128.4°C
• Density: 1.111g/cm³
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 199.079727485
• Heavy Atom Count: 15
• Complexity: 227

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=C(C1=CC=CC=C1F)C2=CC=CC=N2

Technology Process of Pyridine, 2-(1-(2-fluorophenyl)ethenyl-

There total 3 articles about Pyridine, 2-(1-(2-fluorophenyl)ethenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N,N-dimethyl acetamide (127-19-5,116057-81-9) + 2-(2-fluorobenzyl)pyridine (1374650-39-1) → 2-[1-(2-fluorophenyl)vinyl]pyridine (74309-53-8)

Guidance literature:

With sodium persulfate; copper(II) acetate monohydrate; at 120 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ol500655k

Reference yield:

(2-fluorophenyl)(pyridin-2-yl)methanone (6238-65-9) → 2-[1-(2-fluorophenyl)vinyl]pyridine (74309-53-8)

Guidance literature:

DOI:10.1021/ja00536a034

Reference yield:

1-(2-Fluoro-phenyl)-1-pyridin-2-yl-ethanol (125226-31-5) → 2-[1-(2-fluorophenyl)vinyl]pyridine (74309-53-8)

Guidance literature:

DOI:10.1021/ja00536a034

upstream raw materials:

1-(2-Fluoro-phenyl)-1-pyridin-2-yl-ethanol

(2-fluorophenyl)(pyridin-2-yl)methanone

N,N-dimethyl acetamide

2-(2-fluorobenzyl)pyridine

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