2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-(4-morpholinylcarbonyl)-1H -1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-

Base Information

• Chemical Name: 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-(4-morpholinylcarbonyl)-1H -1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-
• CAS No.: 65699-09-4
• Molecular Formula: C₃₁H₂₄Cl₂N₆O₆
• Molecular Weight: 647.474

Synonyms:

Chemical Property of 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-(4-morpholinylcarbonyl)-1H -1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-

Chemical Property:

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Useful:

Technology Process of 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-(4-morpholinylcarbonyl)-1H -1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo-

There total 2 articles about 2H-Isoindole-2-acetamide, N-[[1-[4-chloro-2-(2-chlorobenzoyl)phenyl]-3-(4-morpholinylcarbonyl)-1H -1,2,4-triazol-5-yl]methyl]-1,3-dihydro-1,3-dioxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C17H15Cl2N3O3 (65698-98-8) → N,N-phthaloyl-glycine {2-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-5-(morpholine-4-carbonyl)-2H-[1,2,4]triazol-3-ylmethyl}-amide (65699-09-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / methanol / 96 h / Ambient temperature

2: 1) THF, hexamethylphosphoramide, r.t., 4 h, 2) acetic acid, reflux, 1.5 h

In methanol;

DOI:10.1002/jhet.5570190621

Reference yield:

→ N,N-phthaloyl-glycine {2-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-5-(morpholine-4-carbonyl)-2H-[1,2,4]triazol-3-ylmethyl}-amide (65699-09-4)

Guidance literature:

aus entspr.Phtalylglycylglycylchlorid,HOAc,entspr.'Carbonylhydrazin';

Reference yield:

N,N-phthaloyl-glycine {2-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-5-(morpholine-4-carbonyl)-2H-[1,2,4]triazol-3-ylmethyl}-amide (65699-09-4) → glycine {2-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-5-(morpholine-4-carbonyl)-2H-[1,2,4]triazol-3-ylmethyl}-amide (65699-33-4)

Guidance literature:

With hydrazine hydrate; In ethanol; for 1h; Heating;

DOI:10.1002/jhet.5570190621

upstream raw materials:

C₁₇H₁₅Cl₂N₃O₃

Downstream raw materials:

glycine {2-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-5-(morpholine-4-carbonyl)-2H-[1,2,4]triazol-3-ylmethyl}-amide

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