1H-1,2,4-Triazole-3-carboxamide, 5-[[(2-amino-4-methyl-1-oxopentyl)amino]methyl]-1-[4-chloro-2-(2-chloro benzoyl)phenyl]-N,N-dimethyl-, (S)-

Base Information

Chemical Name:1H-1,2,4-Triazole-3-carboxamide, 5-[[(2-amino-4-methyl-1-oxopentyl)amino]methyl]-1-[4-chloro-2-(2-chloro benzoyl)phenyl]-N,N-dimethyl-, (S)-
CAS No.:65699-24-3
Molecular Formula:C₂₅H₂₈Cl₂N₆O₃
Molecular Weight:531.442
Hs Code.:

Synonyms:

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Chemical Property of 1H-1,2,4-Triazole-3-carboxamide, 5-[[(2-amino-4-methyl-1-oxopentyl)amino]methyl]-1-[4-chloro-2-(2-chloro benzoyl)phenyl]-N,N-dimethyl-, (S)-

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Technology Process of 1H-1,2,4-Triazole-3-carboxamide, 5-[[(2-amino-4-methyl-1-oxopentyl)amino]methyl]-1-[4-chloro-2-(2-chloro benzoyl)phenyl]-N,N-dimethyl-, (S)-

There total 10 articles about 1H-1,2,4-Triazole-3-carboxamide, 5-[[(2-amino-4-methyl-1-oxopentyl)amino]methyl]-1-[4-chloro-2-(2-chloro benzoyl)phenyl]-N,N-dimethyl-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65699-22-1
1-[4-Chloro-2-(2-chloro-benzoyl)-phenyl]-5-{[(S)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-4-methyl-pentanoylamino]-methyl}-1H-[1,2,4]triazole-3-carboxylic acid dimethylamide

: 65699-24-3
2',5-dichloro-2-(3-dimethylcarbamoyl-5-L-leucylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;
DOI:10.1002/jhet.5570190621

Reference yield:

: 50330-59-1
8-chloro-6-(2-chloro-phenyl)-4H-benzo[f][1,2,4]triazolo[1,5-a][1,4]diazepine-2-carboxylic acid dimethylamide

: 65699-24-3
2',5-dichloro-2-(3-dimethylcarbamoyl-5-L-leucylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HBr / Heating

2: benzene; dimethylformamide / 4 h / Ambient temperature

3: hydrazine hydrate / ethanol / 1 h / Heating

With hydrogen bromide; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621

Reference yield:

: 65698-99-9
N,N-dimethyl 2-amino-2-(2-(2-chlorobenzoyl)-5-chlorophenylazo)acetamide

: 65699-24-3
2',5-dichloro-2-(3-dimethylcarbamoyl-5-L-leucylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / K₂CO₃ / tetrahydrofuran; dimethylformamide / Ambient temperature; overnight

2: 30percent HBr/acetic acid / 2 h / Ambient temperature

3: benzene; dimethylformamide / 4 h / Ambient temperature

4: hydrazine hydrate / ethanol / 1 h / Heating

With hydrogen bromide; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621