Bicyclo[5.2.0]nonan-8-one

Base Information

Chemical Name:Bicyclo[5.2.0]nonan-8-one
CAS No.:65811-21-4
Molecular Formula:C9H14O
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID40508070
Nikkaji Number:J2.048.726G

Synonyms:Bicyclo[5.2.0]nonan-8-one;65811-21-4;SCHEMBL13193340;DTXSID40508070;AKOS017975486

Suppliers and Price of Bicyclo[5.2.0]nonan-8-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Bicyclo[5.2.0]nonan-8-one

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:138.104465066
Heavy Atom Count:10
Complexity:151

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2CC(=O)C2CC1

Technology Process of Bicyclo[5.2.0]nonan-8-one

There total 1 articles about Bicyclo[5.2.0]nonan-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 79894-67-0
4-Dimethylamino-benzenesulfonic acid (1R,2S)-2-ethynyl-cycloheptyl ester

: 14377-11-8
1-acetyl-1-cycloheptene

: 65811-21-4
bicyclo[5.2.0]nonan-8-one

Guidance literature:: With sulfuric acid; at 0 - 20 ℃; for 0.75h; Product distribution;
DOI:10.1055/s-1981-29505

Reference yield:

: 65811-21-4
bicyclo[5.2.0]nonan-8-one

: 65811-17-8
Bicyclo<5.2.0>non-1-en

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol

2: (i) MeSO₂Cl, Py, CH₂Cl₂, (ii) KOtBu, DMSO

3: KOtBu, DMSO

With sodium tetrahydroborate; potassium tert-butylate; dimethyl sulfoxide; In methanol;
DOI:10.1021/ja00470a027