Technology Process of Cyclopentanol, 2-phenyl-3-(phenylsulfonyl)-
There total 5 articles about Cyclopentanol, 2-phenyl-3-(phenylsulfonyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran;
for 24h;
from -78 to 25 deg C;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70 percent / pyridinium chlorochromate, sodium carbonate / CH2Cl2 / 0.17 h
2: 8.0 g / benzyltriethylammonium chloride, 50 percent NaOH / CH2Cl2 / 1 h
3: 87 percent / MCPBA / CH2Cl2 / Heating
4: 75 percent / LDA / tetrahydrofuran / 24 h / from -78 to 25 deg C
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 84 percent / KOH / methanol
2: 70 percent / pyridinium chlorochromate, sodium carbonate / CH2Cl2 / 0.17 h
3: 8.0 g / benzyltriethylammonium chloride, 50 percent NaOH / CH2Cl2 / 1 h
4: 87 percent / MCPBA / CH2Cl2 / Heating
5: 75 percent / LDA / tetrahydrofuran / 24 h / from -78 to 25 deg C
With
potassium hydroxide; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane;