Technology Process of Benzoic acid, 4-methoxy-2-methyl-6-(phenylmethoxy)-,
6,8-bis(phenylmethoxy)-1,3-naphthalenediyl ester
There total 13 articles about Benzoic acid, 4-methoxy-2-methyl-6-(phenylmethoxy)-,
6,8-bis(phenylmethoxy)-1,3-naphthalenediyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: K2CO3 / acetone / 72 h / Heating
2: NaOH / ethanol / 1.5 h / Heating
3: thionyl chloride / benzene / 1 h / Heating
4: Et3N / diethyl ether / 4 h
5: 86 percent / silver benzoate, Et3N / 1 h / Heating
6: 55 percent / AcOH, perchloric acid (3 drops) / 0.25 h / Ambient temperature
7: NaH / tetrahydrofuran / 2 h / Ambient temperature
8: tetrahydrofuran / 0.5 h
With
sodium hydroxide; thionyl chloride; perchloric acid; silver benzoate; sodium hydride; potassium carbonate; acetic acid; triethylamine;
In
tetrahydrofuran; diethyl ether; ethanol; acetone; benzene;
DOI:10.1039/P19810002710
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride / benzene / 1 h / Heating
2: Et3N / diethyl ether / 4 h
3: 86 percent / silver benzoate, Et3N / 1 h / Heating
4: 55 percent / AcOH, perchloric acid (3 drops) / 0.25 h / Ambient temperature
5: NaH / tetrahydrofuran / 2 h / Ambient temperature
6: tetrahydrofuran / 0.5 h
With
thionyl chloride; perchloric acid; silver benzoate; sodium hydride; acetic acid; triethylamine;
In
tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/P19810002710
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / K2CO3 / acetone / 48 h / Heating
2: 90 percent / KOH / ethanol / 2 h / Heating
3: thionyl chloride / 2 h / Heating
4: tetrahydrofuran / 0.5 h
With
potassium hydroxide; thionyl chloride; potassium carbonate;
In
tetrahydrofuran; ethanol; acetone;
DOI:10.1039/P19810002710
