Technology Process of Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-,
potassium salt
There total 5 articles about Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-,
potassium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
dichloromethane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Bis(diphenylphosphanyl)amine;
With
sulfur;
In
toluene;
at 110 ℃;
for 12h;
Inert atmosphere;
With
potassium hydroxide;
In
methanol; water;
Inert atmosphere;
DOI:10.1039/c8tc06346j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,1,1,3,3,3-hexamethyl-disilazane / toluene / 12 h / 110 °C / Inert atmosphere
2: sulfur / toluene / 12 h / 110 °C / Inert atmosphere
3: potassium hydroxide / methanol; water / Inert atmosphere
With
sulfur; 1,1,1,3,3,3-hexamethyl-disilazane; potassium hydroxide;
In
methanol; water; toluene;
DOI:10.1039/c8tc02265h
