Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-, potassium salt

Base Information

Chemical Name:Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-, potassium salt
CAS No.:6588-06-3
Molecular Formula:C24H21NP2S2.K
Molecular Weight:487.607
Hs Code.:

Synonyms:

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Chemical Property of Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-, potassium salt

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-, potassium salt

There total 5 articles about Phosphinimidothioic acid, N-(diphenylphosphinothioyl)-P,P-diphenyl-, potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 6588-07-4
bis(diphenylthiophosphinoyl)amine

: 6588-06-3
potassium tetraphenyldithioimidodiphosphinate

Guidance literature:: With potassium hydroxide; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 2960-37-4
Bis(diphenylphosphanyl)amine

: 6588-06-3
potassium tetraphenyldithioimidodiphosphinate

Guidance literature:: Bis(diphenylphosphanyl)amine; With sulfur; In toluene; at 110 ℃; for 12h; Inert atmosphere;

With potassium hydroxide; In methanol; water; Inert atmosphere;
DOI:10.1039/c8tc06346j

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 6588-06-3
potassium tetraphenyldithioimidodiphosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1,1,3,3,3-hexamethyl-disilazane / toluene / 12 h / 110 °C / Inert atmosphere

2: sulfur / toluene / 12 h / 110 °C / Inert atmosphere

3: potassium hydroxide / methanol; water / Inert atmosphere

With sulfur; 1,1,1,3,3,3-hexamethyl-disilazane; potassium hydroxide; In methanol; water; toluene;
DOI:10.1039/c8tc02265h