N-[6-(9-ethoxy-2,5,7,10-tetraoxadodecan-9-yl)-4-oxo-1,4-dihydropyrimidin-2-yl]-2,2-dimethylpropanamide

Base Information

Chemical Name:N-[6-(9-ethoxy-2,5,7,10-tetraoxadodecan-9-yl)-4-oxo-1,4-dihydropyrimidin-2-yl]-2,2-dimethylpropanamide
CAS No.:86944-41-4
Molecular Formula:C₁₉H₃₃N₃O₇
Molecular Weight:415.487
Hs Code.:

Synonyms:Propanamide,N-[6-[1,1-diethoxy-2-[(2-methoxyethoxy)methoxy]ethyl]-1,4-dihydro-4-oxo-2-pyrimidinyl]-2,2-dimethyl-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[6-(9-ethoxy-2,5,7,10-tetraoxadodecan-9-yl)-4-oxo-1,4-dihydropyrimidin-2-yl]-2,2-dimethylpropanamide

Chemical Property:

Density:1.16g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-[6-(9-ethoxy-2,5,7,10-tetraoxadodecan-9-yl)-4-oxo-1,4-dihydropyrimidin-2-yl]-2,2-dimethylpropanamide

There total 3 articles about N-[6-(9-ethoxy-2,5,7,10-tetraoxadodecan-9-yl)-4-oxo-1,4-dihydropyrimidin-2-yl]-2,2-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 86944-38-9
2-pivalamido-6-(1,1-diethoxy-2-hydroxyethyl)-4(1H)-pyrimidinone

: 86944-41-4
2-pivalamido-6-<1,1-diethoxy-2-<(methoxyethoxy)methoxy>ethyl>-4(1H)-pyrimidinone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 24h;
DOI:10.1021/jo00169a001

Reference yield:

: 86944-28-7
2-pivalamido-6-(1-ethoxyvinyl)-4(1H)-pyrimidinone

: 86944-41-4
2-pivalamido-6-<1,1-diethoxy-2-<(methoxyethoxy)methoxy>ethyl>-4(1H)-pyrimidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / MCPBA, BHT / 2 h / Heating

2: 56 percent / iPr₂NEt / CH₂Cl₂ / 24 h / 25 °C

With 2,6-di-tert-butyl-4-methyl-phenol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00169a001

Reference yield:

: 86944-27-6
2-pivalamido-6-(1,1-diethoxyethyl)-4(1H)-pyrimidinone

: 86944-41-4
2-pivalamido-6-<1,1-diethoxy-2-<(methoxyethoxy)methoxy>ethyl>-4(1H)-pyrimidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / toluenesulfonic acid / xylene / 0.25 h / Heating

2: 81 percent / MCPBA, BHT / 2 h / Heating

3: 56 percent / iPr₂NEt / CH₂Cl₂ / 24 h / 25 °C

With 2,6-di-tert-butyl-4-methyl-phenol; o-toluenesulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; xylene;
DOI:10.1021/jo00169a001