3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

Base Information

• Chemical Name: 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE
• CAS No.: 6274-18-6
• Molecular Formula: C8H12N2O2S
• Molecular Weight: 200.261
• Hs Code.: 2935009090
• Mol file: 6274-18-6.mol

Synonyms:Metanilamide,N1,N1-dimethyl- (7CI,8CI);3-Amino-N,N-dimethylbenzenesulfonamide;3-Dimethylsulfamoylaniline;N,N-Dimethyl-3-aminobenzenesulfonamide;NSC 36995;

Chemical Property of 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

Chemical Property:

• Vapor Pressure: 1.37E-05mmHg at 25°C
• Melting Point: 156-158 °C
• Refractive Index: 1.579
• Boiling Point: 367.4 °C at 760 mmHg
• PKA: 3.12±0.10(Predicted)
• Flash Point: 176 °C
• PSA: 71.78000
• Density: 1.273 g/cm³
• LogP: 2.18110
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Amino-N,N-dimethylbenzenesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE

There total 4 articles about 3-AMINO-N,N-DIMETHYL-BENZENESULFONAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

→ 3-amino-N,N-dimethylbenzenesulfonamide (6274-18-6)

Guidance literature:

Reference yield: 80.0%

N,N-dimethyl-3-nitro-benzenesulfonamide (26199-83-7) → 3-amino-N,N-dimethylbenzenesulfonamide (6274-18-6)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol;

Reference yield:

(i-Pr)2 NEt + Me2 NH + 3-nitrobenzenesulphonyl chloride (121-51-7) → 3-amino-N,N-dimethylbenzenesulfonamide (6274-18-6)

Guidance literature:

In dichloromethane; ethyl acetate;

upstream raw materials:

N,N-dimethyl-3-nitro-benzenesulfonamide

3-nitrobenzenesulphonyl chloride

Downstream raw materials:

N,N-Dimethyl-3-trifluoromethanesulfonylamino-benzenesulfonamide

N-(3-(dimethylsulfamoyl)phenyl)-3-methyl-D-valyl-(4R)-4-((7-chloro-4-methoxy-1-isoquinolinyl)oxy)-N-((1R,2S)-1-((cyclopropylsulfonyl)carbamoyl)-2-vinylcyclopropyl)-L-prolinamide

N-(3-(dimethylsulfamoyl)phenyl)-3-methyl-L-valyl-(4R)-4-((7-chloro-4-methoxy-1-isoquinolinyl)oxy)-N-((1R,2S)-1-((cyclopropylsulfonyl)carbamoyl)-2-vinylcyclopropyl)-L-prolinamide

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