3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium

Base Information

Chemical Name:3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium
CAS No.:66074-01-9
Molecular Formula:C14H8Cl2N2O6S2
Molecular Weight:435.265
Hs Code.:

Synonyms:SCHEMBL2202054

Suppliers and Price of 3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:433.9200837
Heavy Atom Count:26
Complexity:692

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1S(=O)(=O)C2=NO[N+](=C2S(=O)(=O)C3=CC=C(C=C3)Cl)[O-])Cl

Technology Process of 3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium

There total 6 articles about 3,4-Bis[(4-chlorophenyl)sulfonyl]-2-oxido-1,2,5-oxadiazol-2-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3405-89-8
2-(4-chloro-phenylsulfonyl)acetic acid

: 66074-01-9
3,4-bis(4-chlorobenzene-1-sulfonyl)furoxan

Guidance literature:: With nitric acid; In acetic acid;
DOI:10.1039/jr9640000904

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 66074-01-9
3,4-bis(4-chlorobenzene-1-sulfonyl)furoxan

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium / toluene / 130 °C / Schlenk technique; Inert atmosphere

1.2: 24 h / Reflux; Schlenk technique; Inert atmosphere

2.1: oxone||potassium monopersulfate triple salt / water; ethanol / 20 °C / Schlenk technique; Inert atmosphere

3.1: sodium hydroxide / water; tetrahydrofuran / 20 °C / Schlenk technique; Inert atmosphere

3.2: Schlenk technique; Inert atmosphere

4.1: nitric acid; acetic acid / 0 - 140 °C / Schlenk technique; Inert atmosphere

With oxone||potassium monopersulfate triple salt; nitric acid; sodium; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1021/acs.orglett.0c00062

Reference yield:

: 52377-68-1
ethyl 2-(p-chlorophenylthio)acetate

: 66074-01-9
3,4-bis(4-chlorobenzene-1-sulfonyl)furoxan

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxone||potassium monopersulfate triple salt / water; ethanol / 20 °C / Schlenk technique; Inert atmosphere

2.1: sodium hydroxide / water; tetrahydrofuran / 20 °C / Schlenk technique; Inert atmosphere

2.2: Schlenk technique; Inert atmosphere

3.1: nitric acid; acetic acid / 0 - 140 °C / Schlenk technique; Inert atmosphere

With oxone||potassium monopersulfate triple salt; nitric acid; acetic acid; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/acs.orglett.0c00062