1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Base Information

Chemical Name:1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride
CAS No.:602-10-8
Molecular Formula:C15H6 Cl N O5
Molecular Weight:315.669
Hs Code.:
NSC Number:117935
DSSTox Substance ID:DTXSID80297774
Nikkaji Number:J29.724K
Wikidata:Q82039143
Mol file:602-10-8.mol

Synonyms:602-10-8;1-nitro-9,10-dioxoanthracene-2-carbonyl chloride;1-NITRO-9,10-DIOXO-9,10-DIHYDROANTHRACENE-2-CARBONYL CHLORIDE;NSC117935;1-NITRO-2-ANTHRAQUINONECARBONYL CHLORIDE;SCHEMBL11776076;DTXSID80297774;AKOS000592631;NSC-117935;2-Anthraquinonecarbonyl chloride, 1-nitro-;2-Anthroyl chloride,10-dihydro-1-nitro-9,10-dioxo-;2-Anthroyl chloride, 9,10-dihydro-1-nitro-9,10-dioxo-;2-Anthracenecarbonyl chloride,10-dihydro-1-nitro-9,10-dioxo-;9,10-Dihydro-1-nitro-9,10-dioxoanthracene-2-carbonyl chloride;2-Anthracenecarbonyl chloride, 9,10-dihydro-1-nitro-9,10-dioxo-

Suppliers and Price of 1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Chemical Property:

Vapor Pressure:7.36E-12mmHg at 25°C
Boiling Point:543.2°C at 760 mmHg
Flash Point:282.3°C
PSA：97.03000
Density:1.599g/cm³
LogP:3.27240
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:314.9934500
Heavy Atom Count:22
Complexity:543

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C(=C(C=C3)C(=O)Cl)[N+](=O)[O-]

Technology Process of 1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

There total 4 articles about 1-Nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 128-67-6
1-nitroanthraquinone-2-carboxylic acid

: 602-10-8
1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In benzene; at 80 ℃; for 3h;
DOI:10.1023/A:1013003122428

Reference yield:

: 84-54-8
2-methylanthracene-9,10-dione

: 602-10-8
1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; potassium nitrate / 5 - 20 °C

2: sulfuric acid; sodium dichromate / water / 11 h / 90 °C / Cooling with ice

3: thionyl chloride / chlorobenzene / 4 h / 120 °C

With thionyl chloride; sodium dichromate; sulfuric acid; potassium nitrate; In water; chlorobenzene;
DOI:10.3390/molecules25071672

Reference yield:

: 129-15-7
1-nitro-2-methylanthraquinone

: 602-10-8
1-nitro-9,10-dioxo-9,10-dihydroanthracene-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; sodium dichromate / water / 11 h / 90 °C / Cooling with ice

2: thionyl chloride / chlorobenzene / 4 h / 120 °C

With thionyl chloride; sodium dichromate; sulfuric acid; In water; chlorobenzene;
DOI:10.3390/molecules25071672