4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULFONYL]PHENOL

Base Information

• Chemical Name: 4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULFONYL]PHENOL
• CAS No.: 3636-29-1
• Molecular Formula: C12H8Cl2O4S
• Molecular Weight: 319.165
• Hs Code.: 2908999090
• Mol file: 3636-29-1.mol

Synonyms:4-chloro-2-[(5-chloro-2-hydroxyphenyl)sulfonyl]phenol;5,2'-dihydroxydiphenyl sulfone;4,4'-dichloro-2,2'-sulfonyl-di-phenol;bis-2-hydroxy-5-chlorophenyl sulfone;2,5'-dichlorodiphenyl sulfone;Bis-(5-chlor-2-hydroxy-phenyl)-sulfon;4,4'-Dichlor-2,2'-sulfonyl-di-phenol;

Chemical Property of 4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULFONYL]PHENOL

Chemical Property:

• Melting Point: 188oC
• Boiling Point: 534.7°Cat760mmHg
• Flash Point: 277.2°C
• PSA: 82.98000
• Density: 1.607g/cm³
• LogP: 4.31820

Purity/Quality:

99% ^*data from raw suppliers

4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULPHONYL]PHENOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULFONYL]PHENOL

There total 3 articles about 4-CHLORO-2-[(5-CHLORO-2-HYDROXYPHENYL)SULFONYL]PHENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.7%

4-chloro-phenol (106-48-9,82344-39-6) → bis-2-hydroxy-5-chlorophenyl sulfone (3636-29-1)

Guidance literature:

With sulfuric acid; In chlorobenzene; at 140 - 170 ℃; for 3h;

Reference yield:

2,2'-sulfoxide-bis(4-chlorophenol) (29097-31-2) → bis-2-hydroxy-5-chlorophenyl sulfone (3636-29-1)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/ja01218a029

Reference yield:

4,4'-dichloro-2,2'-thiodiphenol (97-24-5) → bis-2-hydroxy-5-chlorophenyl sulfone (3636-29-1)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/ja01218a029

upstream raw materials:

2,2'-sulfoxide-bis(4-chlorophenol)

4,4'-dichloro-2,2'-thiodiphenol

4-chloro-phenol

Downstream raw materials:

6,6'-diamino-4,4'-dichloro-2,2'-sulfonyl-di-phenol

5,5'-dichloro-3,3'-dinitro-2,2'-dihydroxydiphenyl sulfone

Refernces