Disulfide, (4-nitrophenyl)methyl phenylmethyl

Base Information

• Chemical Name: Disulfide, (4-nitrophenyl)methyl phenylmethyl
• CAS No.: 66138-10-1
• Molecular Formula: C14H13NO2S2
• Molecular Weight: 291.395
• Mol file: 66138-10-1.mol

Synonyms:

Chemical Property of Disulfide, (4-nitrophenyl)methyl phenylmethyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Disulfide, (4-nitrophenyl)methyl phenylmethyl

There total 2 articles about Disulfide, (4-nitrophenyl)methyl phenylmethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

benzyl chloride (100-44-7) + S-(4-nitrophenylmethyl)thioacetate (170640-75-2) → 1-benzyl-2-(4-nitrobenzyl)disulfane (66138-10-1)

Guidance literature:

With caesium carbonate; sodium thiosulfate; In water; at 70 ℃; for 24h; Schlenk technique; Green chemistry;

DOI:10.1002/adsc.202000851

Reference yield:

→ 1-benzyl-2-(4-nitrobenzyl)disulfane (66138-10-1)

Guidance literature:

Kalium p-nitrobenzylthiosulfat, SrNO3, Benzylthiol 2;

Reference yield:

1-benzyl-2-(4-nitrobenzyl)disulfane (66138-10-1) → bis(4-nitrobenzyl) sulfide (1835-71-8)

Guidance literature:

With hexaethylphosphoric triamide; In benzene; Ambient temperature;

DOI:10.1021/ja00739a014

upstream raw materials:

benzyl chloride

S-(4-nitrophenylmethyl)thioacetate

Downstream raw materials:

bis(4-nitrobenzyl) sulfide