Aids001181

Base Information

• Chemical Name: Aids001181
• CAS No.: 121055-66-1
• Molecular Formula: C₂₃H₄₀N₆O₃Si₂
• Molecular Weight: 504.78
• Mol file: 121055-66-1.mol

Synonyms:

Chemical Property of Aids001181

Chemical Property:

• Vapor Pressure: 2.07E-14mmHg at 25°C
• Boiling Point: 601.2°Cat760mmHg
• Flash Point: 317.4°C
• PSA: 111.87000
• Density: 1.13g/cm³
• LogP: 6.12728

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Aids001181

There total 1 articles about Aids001181 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium cyanide (143-33-9,25596-52-5) + 9-(2,5-di-O-tert-butyldimethylsilyl-β-D-erythro-pentofuran-3-ulosyl)adenosine (86734-95-4) → 9-<2',5'-bis-O-(tert-butyldimethylsilyl)-3'-C-cyano-3'-deoxy-β-D-xylo-pentofuranosyl>adenine (121055-66-1)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jm00128a011

Reference yield: 67.0%

9-<2',5'-bis-O-(tert-butyldimethylsilyl)-3'-C-cyano-3'-deoxy-β-D-xylo-pentofuranosyl>adenine (121055-66-1) → 9-(3'-C-cyano-3'-deoxy-β-D-xylo-pentofuranosyl)adenine (121153-18-2)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.333333h; Ambient temperature;

DOI:10.1021/jm00128a011

upstream raw materials:

sodium cyanide

9-(2,5-di-O-tert-butyldimethylsilyl-β-D-erythro-pentofuran-3-ulosyl)adenosine

Downstream raw materials:

9-(3'-C-cyano-3'-deoxy-β-D-xylo-pentofuranosyl)adenine

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