tripitramine

Base Information

• Chemical Name: tripitramine
• CAS No.: 152429-64-6
• Molecular Formula: C64H77 N13 O6
• Molecular Weight: 1124.3797
• Mol file: 152429-64-6.mol

Synonyms:Tripitramine

Chemical Property of tripitramine

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 219.12000
• Density: 1.232g/cm³
• LogP: 10.22450

Purity/Quality:

TRIPITRAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tripitramine

There total 7 articles about tripitramine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C71H83N13O6 (152429-68-0) → Tripitramine (152429-64-6)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; at 50 ℃; for 12h; under 3800 Torr;

DOI:10.1021/jm00075a032

Reference yield: 19.0%

11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one (28797-48-0) + 1,24-bis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-8,17-dimethyl-1,8,17,24-tetraazatetracosane (152429-63-5) → Tripitramine (152429-64-6) + 1,1,24,24-tetrakis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-8,17-dimethyl-1,8,17,24-tetraazatetracosane

Guidance literature:

In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1021/jm00046a021

Reference yield: 10.0%

11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one (28797-48-0) + N,N'-bis(6-aminohexyl)-N,N'-dimethyl-1,8-octanediamine (115962-75-9) → 1,24-bis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-8,17-dimethyl-1,8,17,24-tetraazatetracosane (152429-63-5) + Tripitramine (152429-64-6) + 1,1,24,24-tetrakis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-8,17-dimethyl-1,8,17,24-tetraazatetracosane

Guidance literature:

In N,N-dimethyl-formamide; for 36h; Ambient temperature;

DOI:10.1021/jm00046a021

upstream raw materials:

C₇₁H₈₃N₁₃O₆

11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one

N,N'-bis(6-aminohexyl)-N,N'-dimethyl-1,8-octanediamine

1,24-bis<<(5,11-dihydro-6-oxo-6H-pyrido<2,3-b><1,4>benzodiazepin-11-yl)carbonyl>methyl>-8,17-dimethyl-1,8,17,24-tetraazatetracosane

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