2,2-Dichloro-1-phenylpentan-1-one

Base Information

Chemical Name:2,2-Dichloro-1-phenylpentan-1-one
CAS No.:66255-86-5
Molecular Formula:C11H12Cl2O
Molecular Weight:231.122
Hs Code.:
DSSTox Substance ID:DTXSID80496689
Nikkaji Number:J336.256F
Wikidata:Q82345712

Synonyms:2,2-dichloro-1-phenylpentan-1-one;66255-86-5;2,2-dichloro-1-phenyl-1-pentanone;DTXSID80496689

Suppliers and Price of 2,2-Dichloro-1-phenylpentan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2-Dichloro-1-phenylpentan-1-one

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:230.0265204
Heavy Atom Count:14
Complexity:196

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(C(=O)C1=CC=CC=C1)(Cl)Cl

Technology Process of 2,2-Dichloro-1-phenylpentan-1-one

There total 5 articles about 2,2-Dichloro-1-phenylpentan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 130400-99-6
N-(2,2-Dichloro-1-phenyl-1-pentylidene)isopropylamine

: 66255-86-5
2,2-Dichloro-1-phenyl-1-pentanone

Guidance literature:: With hydrogenchloride; In dichloromethane; for 2h; Heating;

Reference yield: 61.0%

: 1009-14-9
phenyl butyl ketone

: 66255-86-5
2,2-Dichloro-1-phenyl-1-pentanone

Guidance literature:: With sulfuryl dichloride; In neat (no solvent); at 80 ℃; for 72h;
DOI:10.1016/j.tetlet.2021.153335

Reference yield:

: 2648-61-5
2,2-dichloroacetophenone

: 66255-86-5
2,2-Dichloro-1-phenyl-1-pentanone

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / TiCl₄ / benzene; pentane / 1) 1 h, ice-bath, 2) 1.5 h, rt

2: 1) LDA / 1) THF, hexane, 20 min, 0 deg C, 2) 0 deg C, 1 h; then rt, 2 h

3: 79 percent / aq. 2N HCl / CH₂Cl₂ / 2 h / Heating

With hydrogenchloride; titanium tetrachloride; lithium diisopropyl amide; In dichloromethane; pentane; benzene;