N-desmethylnefopam

Base Information

Chemical Name:N-desmethylnefopam
CAS No.:46868-19-3
Molecular Formula:C16H17NO
Molecular Weight:239.317
Hs Code.:
Mol file:46868-19-3.mol

Synonyms:nor-nefopam;1H-2,5-Benzoxazocine,3,4,5,6-tetrahydro-1-phenyl;desmethyl nefopam;

Suppliers and Price of N-desmethylnefopam

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-DesmethylNefopam
25mg
$ 275.00

American Custom Chemicals Corporation
N-DESMETHYLNEFOPAM 95.00%
5MG
$ 499.88

Total 2 raw suppliers

Chemical Property of N-desmethylnefopam

Chemical Property:

Vapor Pressure:4.4E-06mmHg at 25°C
Boiling Point:383.4°Cat760mmHg
Flash Point:157.1°C
PSA：21.26000
Density:1.073g/cm³
LogP:3.22460

Purity/Quality:

≥90% ^*data from raw suppliers

N-DesmethylNefopam ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-desmethylnefopam

There total 10 articles about N-desmethylnefopam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 84940-28-3
1-phenyl-3,4,5,6-tetrahydro-1H-2,5-benzoxazocine-5-carbonitrile

: 46868-19-3
N-Desmethylnefopam

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1071/CH02097

Reference yield: 88.0%

: 47205-41-4
1-phenyl-1,3,4,6-tetrahydro-1H-2,5-benzoxazocine-5-propanenitrile

: 46868-19-3
N-Desmethylnefopam

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1071/CH02097

Reference yield:

: 147678-38-4
2-(2'-hydroxyethyl)amino-5-phenyl-2,5-dihydro-3,4-benzofuran

: 46868-19-3
N-Desmethylnefopam

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / 10percent Pd/C / methanol / 1.5 h / 2327.2 Torr

2: p-TsOH*H₂O / toluene / 3 h / Heating

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; toluene;
DOI:10.1002/jps.2600820312