5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol

Base Information

Chemical Name:5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol
CAS No.:66465-77-8
Molecular Formula:C₁₃H₂₂O₂
Molecular Weight:210.316
Hs Code.:
DSSTox Substance ID:DTXSID90705739

Synonyms:66465-77-8;5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol;SCHEMBL11356387;DTXSID90705739

Suppliers and Price of 5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:210.161979940
Heavy Atom Count:15
Complexity:287

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCC(C(C1=CCC(C)O)(C)C)O

Technology Process of 5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol

There total 2 articles about 5-(3-Hydroxybutylidene)-4,6,6-trimethylcyclohex-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66465-76-7,70429-51-5,73174-82-0,108342-23-0
(S)-2,9-diacetoxy-4,6,8-megastigmatriene

: 66465-77-8
(S)-4,6-megastigmadiene-2,9-diol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;
DOI:10.1016/S0040-4020(01)90549-6

Reference yield:

: 67504-50-1
(-)-(2S)-2-hydroxy-β-ionone

: 66465-77-8
(S)-4,6-megastigmadiene-2,9-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 2.14 g / p-TsOH*H₂O / 0.67 h / Heating

2: 1.66 g / LAH / diethyl ether / 1 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)90549-6