3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine

Base Information

Chemical Name:3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine
CAS No.:103139-94-2
Molecular Formula:C₁₂H₁₃N₅
Molecular Weight:227.269
Hs Code.:
UNII:201ZX05138
DSSTox Substance ID:DTXSID60145668
Nikkaji Number:J456.402B
Wikidata:Q27894163
Mol file:103139-94-2.mol

Synonyms:3,5,8-trimethylimidazo(4,5-f)quinoxalin-2-amine;5,8-diMeIQX

Suppliers and Price of 3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine

Chemical Property:

Vapor Pressure:6.77E-09mmHg at 25°C
Boiling Point:467°Cat760mmHg
Flash Point:236.2°C
PSA：70.35000
Density:1.42g/cm³
LogP:1.64560
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:227.11709544
Heavy Atom Count:17
Complexity:297

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C3=NC(=CN=C13)C)N=C(N2C)N

Technology Process of 3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine

There total 9 articles about 3,5,8-Trimethylimidazo(4,5-f)quinoxalin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 138336-29-5
2-(N-benzylamino)-3,5,8-trimethylimidazo<4,5-f>quinoxaline

: 103139-94-2
3,5,8-trimethyl-3H-imidazo<4,5-f>quinoxalin-2-amine

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 120h; Heating;
DOI:10.1021/jo00031a017

Reference yield:

: 138336-15-9
2-(methylthio)-3,5,8-trimethylimidazo<4,5-f>quinoxaline

: 103139-94-2
3,5,8-trimethyl-3H-imidazo<4,5-f>quinoxalin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 79.3 percent / aq. KMnO₄, glacial acetic acid / 1 h / Ambient temperature

2: 91 percent / 51 h / 145 - 150 °C

3: 83 percent / ammonium formate / 10percent Pd/C / methanol / 120 h / Heating

With potassium permanganate; ammonium formate; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00031a017

Reference yield:

: 138336-23-9
2-(methylsulfonyl)-3,5,8-trimethylimidazo<4,5-f>quinoxaline

: 103139-94-2
3,5,8-trimethyl-3H-imidazo<4,5-f>quinoxalin-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 51 h / 145 - 150 °C

2: 83 percent / ammonium formate / 10percent Pd/C / methanol / 120 h / Heating

With ammonium formate; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00031a017