Technology Process of (1E,3E,7E,11E)-1,7,11-Trimethyl-4-isopropyl-1,3,7,11-cyclotetradecatetrene
There total 9 articles about (1E,3E,7E,11E)-1,7,11-Trimethyl-4-isopropyl-1,3,7,11-cyclotetradecatetrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; titanium tetrachloride; zinc;
In
1,2-dimethoxyethane;
for 3h;
Heating;
DOI:10.1080/00397919408012651
- Guidance literature:
-
With
zinc copper; magnesium;
In
ethanol;
for 72h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: LDA / 1.) THF, hexane, -78 deg C, 40 min, 2.) THF, hexane, a) -78 deg C, 2 h, b) RT, overnight
2: K2CO3 / methanol / 1 h / Ambient temperature
3: 90 percent / MnO2, Na2CO3 / CH2Cl2 / 4 h / Ambient temperature
4: 72 percent / TiCl4, Zn, pyridine / 1,2-dimethoxy-ethane / 3 h / Heating
With
pyridine; manganese(IV) oxide; titanium tetrachloride; sodium carbonate; potassium carbonate; zinc; lithium diisopropyl amide;
In
methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1080/00397919408012651
