protoporphyrin IX monomethyl ester

Base Information

Chemical Name:protoporphyrin IX monomethyl ester
CAS No.:16053-68-2
Molecular Formula:C₃₅H₃₆N₄O₄
Molecular Weight:576.695
Hs Code.:
Mol file:16053-68-2.mol

Synonyms:2,18-Porphinedipropionicacid, 3,7,12,17-tetramethyl-8,13-divinyl-, 18-methyl ester (8CI);21H,23H-Porphine-2,18-dipropanoic acid, 7,12-diethenyl-3,8,13,17-tetramethyl-, a2-methyl ester (9CI)

Suppliers and Price of protoporphyrin IX monomethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of protoporphyrin IX monomethyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:1073.5°Cat760mmHg
Flash Point:603°C
PSA：119.90000
Density:1.231g/cm³
LogP:4.32470

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of protoporphyrin IX monomethyl ester

There total 5 articles about protoporphyrin IX monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 137053-80-6
7-(2-t-Butoxycarbonylethyl)-6-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-2,4-divinylporphyrin

: 16053-68-2
7-(2-Carboxyethyl)-6-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-2,4-divinylporphyrin

Guidance literature:: With trifluoroacetic acid; for 0.25h; Ambient temperature;

Reference yield:

: 137053-75-9
2,4-Diacetyl-7-(2-t-butoxycarbonylethyl)-6-(2-carboxyethyl)-1,3,5,8-tetramethylporphyrin

: 16053-68-2
7-(2-Carboxyethyl)-6-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-2,4-divinylporphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / diethyl ether

2: 90 percent / NaBH₄ / CH₂Cl₂; methanol / 1 h / 0 °C

3: 85 percent / toluene-p-sulphonic acid monohydrate / 1,2-dichloro-benzene / 100 °C

4: 95 percent / TFA / 0.25 h / Ambient temperature

With sodium tetrahydroborate; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane; 1,2-dichloro-benzene;

Reference yield:

: 137053-78-2
(2-t-Butoxycarbonylethyl)-2,4-bis-(1-hydroxyethyl)-6-(2-methoxycarbonylethyl)-1,3,5,8-tetramethylporphyrin

: 16053-68-2
7-(2-Carboxyethyl)-6-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-2,4-divinylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / toluene-p-sulphonic acid monohydrate / 1,2-dichloro-benzene / 100 °C

2: 95 percent / TFA / 0.25 h / Ambient temperature

With toluene-4-sulfonic acid; trifluoroacetic acid; In 1,2-dichloro-benzene;