2-Hydroxy-5-methyl-3-nitrobenzaldehyde

Base Information

Chemical Name:2-Hydroxy-5-methyl-3-nitrobenzaldehyde
CAS No.:66620-31-3
Molecular Formula:C8H7NO4
Molecular Weight:181.148
Hs Code.:
DSSTox Substance ID:DTXSID80408429
Nikkaji Number:J1.574.236D
Wikidata:Q82213908

Synonyms:2-hydroxy-5-methyl-3-nitrobenzaldehyde;66620-31-3;2-hydroxy-5-methyl-3-nitro-benzaldehyde;2-hydroxy-3-nitro-5-methylbenzaldehyde;SCHEMBL10013940;3-nitro-5-methyl-salicylaldehyde;DTXSID80408429;AKOS005376428;AE-848/30539045

Suppliers and Price of 2-Hydroxy-5-methyl-3-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Hydroxy-5-methyl-3-nitrobenzaldehyde

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:181.03750770
Heavy Atom Count:13
Complexity:213

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)[N+](=O)[O-])O)C=O

Technology Process of 2-Hydroxy-5-methyl-3-nitrobenzaldehyde

There total 4 articles about 2-Hydroxy-5-methyl-3-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 613-84-3
2-hydroxy-5-methylbenzaldehyde

: 66620-31-3
2-hydroxy-5-methyl-3-nitro-benzaldehyde

Guidance literature:: With nitric acid; at 0 ℃;
DOI:10.1021/jo00244a038

Reference yield:

: 91-04-3
2,6-bis(hydroxymethyl)-4-methylphenol

: 66620-31-3
2-hydroxy-5-methyl-3-nitro-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous NaNO₂; aqueous HCl / 20 °C

2: aqueous NaOH

With hydrogenchloride; sodium hydroxide; sodium nitrite;
DOI:10.1007/BF00898854

Reference yield:

: 4383-07-7
2-hydroxymethyl-4-methylphenol

: 66620-31-3
2-hydroxy-5-methyl-3-nitro-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous NaNO₂; glacial acetic acid / 20 °C

2: aqueous NaOH

With sodium hydroxide; acetic acid; sodium nitrite;
DOI:10.1007/BF00898854