4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline

Base Information

Chemical Name:4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline
CAS No.:666830-58-6
Molecular Formula:C27H23NO
Molecular Weight:377.486
Hs Code.:
DSSTox Substance ID:DTXSID10708065

Synonyms:DTXSID10708065;JRXWOCIYAKMCGO-UHFFFAOYSA-N;4-diphenylamino-4'-methoxystilbene;4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline

Suppliers and Price of 4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline

Chemical Property:

XLogP3:7.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:377.177964357
Heavy Atom Count:29
Complexity:457

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=CC2=CC=C(C=C2)N(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline

There total 5 articles about 4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1145-93-3
diethyl 4-methoxybenzylphosphonate

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 666830-58-6
(E)-4-(4-methoxystyryl)-N,N-diphenylaniline

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 8.16667h;
DOI:10.1039/c2nj40374a

Reference yield: 61.3%

: diethyl-4-methoxybenzyl phosphonate

: 4181-05-9
4-(diphenylamino)benzaldehyde

: 666830-58-6
(E)-4-(4-methoxystyryl)-N,N-diphenylaniline

Guidance literature:: With sodium methylate; acetic acid; In N-methyl-acetamide; methanol; water;

Reference yield:

: 38186-51-5
diethyl (4-bromobenzyl)phosphonate

: 666830-58-6
(E)-4-(4-methoxystyryl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: NaO-tBu; DPPF; Pd₂(dba)3 / toluene

With 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; sodium hydride; sodium t-butanolate; In N,N-dimethyl-formamide; toluene; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo035462k