1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

Base Information

• Chemical Name: 1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde
• CAS No.: 83174-90-7
• Molecular Formula: C7H8N2O3
• Molecular Weight: 168.152
• Hs Code.: 2933599090
• Mol file: 83174-90-7.mol

Synonyms:1,3-Dimethyl-6-formyluracil;1,3-DIMETHYL-2,6-DIOXO-1,2,3,6-TETRAHYDROPYRIMIDINE-4-CARBALDEHYDE;1,3-dimethylorotaldehyde;4-Pyrimidinecarboxaldehyde,1,2,3,6-tetrahydro-1,3-dimethyl-2,6-dioxo;1,3-DiMe-6-FormU;

Chemical Property of 1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

Chemical Property:

• Vapor Pressure: 0.00551mmHg at 25°C
• Boiling Point: 274.1°Cat760mmHg
• Flash Point: 122.6°C
• PSA: 61.07000
• Density: 1.408g/cm³
• LogP: -1.10350

Purity/Quality:

1,3-DIMETHYL-2,6-DIOXO-1,2,3,6-TETRAHYDROPYRIMIDINE-4-CARBALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde

There total 8 articles about 1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,3-dimethylorotaldehyde diethyl acetal (83174-91-8) → 1,3-dimethyl-6-formyluracil (83174-90-7)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; for 3h; Heating;

DOI:10.1021/ja00387a047

Reference yield:

6-(2-dimethylaminovinyl)-1,3-dimethyluracil (116705-39-6) → 1,3-dimethyl-6-formyluracil (83174-90-7)

Guidance literature:

With sodium periodate; In tetrahydrofuran; chloroform; water; at 20 ℃; for 4h;

Reference yield:

1,3,6-trimethyluracil (13509-52-9) → 1,3-dimethyl-6-formyluracil (83174-90-7)

Guidance literature:

With selenium(IV) oxide; In acetic acid; at 100 ℃; for 4h;

upstream raw materials:

1,3,6-trimethyluracil

1,3-dimethylorotaldehyde diethyl acetal

6-Dimethoxymethyl-1,3-dimethyl-1H-pyrimidine-2,4-dione

6-Methyluracil

Downstream raw materials:

1,3-dimethyluracil

6-[Hydroxy-(5-methyl-furan-2-yl)-methyl]-1,3-dimethyl-1H-pyrimidine-2,4-dione

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