5-(2,4-dioxopyrimidin-1-yl)-3,4-dihydroxy-oxolane-2-carboxylic acid

Base Information

• Chemical Name: 5-(2,4-dioxopyrimidin-1-yl)-3,4-dihydroxy-oxolane-2-carboxylic acid
• CAS No.: 3415-07-4
• Molecular Formula: C9H10 N2 O7
• Molecular Weight: 0
• Mol file: 3415-07-4.mol

Synonyms:Ribofuranuronicacid, 1-deoxy-1-(3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl)- (6CI,7CI);Ribofuranuronic acid, 1-deoxy-1-(3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl)-, b-D- (8CI); NSC 315827;Uridine-5'-carboxylic acid

Chemical Property of 5-(2,4-dioxopyrimidin-1-yl)-3,4-dihydroxy-oxolane-2-carboxylic acid

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 141.85000
• Density: 1.851g/cm³
• LogP: -2.75960

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(2,4-dioxopyrimidin-1-yl)-3,4-dihydroxy-oxolane-2-carboxylic acid

There total 3 articles about 5-(2,4-dioxopyrimidin-1-yl)-3,4-dihydroxy-oxolane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N1-(tert-Butyl 2,3-O-isopropylidene-β-D-ribofuranosyluronate)uracil (92985-14-3) → 1-deoxy-1-<3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl>-β-D-ribofuranuronic acid (3415-07-4)

Guidance literature:

With acetic acid; for 5h; Heating;

Reference yield:

→ 1-<β-D-Arabinofuranosyluronsaeure>-uracil (3415-07-4)

Guidance literature:

1-β-D-Arabinofuranosyl-uracil u. O2(Pt) in wss. NaHCO3 b. 50-60grad;

Reference yield:

→ 1-deoxy-1-<3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl>-β-D-ribofuranuronic acid (3415-07-4)

Guidance literature:

Uridin, wss. NaHCO3 + Na2CO3 (pH 8.8), O2/Pt (80grad, 22 h);

upstream raw materials:

N¹-(tert-Butyl 2,3-O-isopropylidene-β-D-ribofuranosyluronate)uracil

Downstream raw materials:

N-<2-(3-cyclohexylureido)ethyl>-1-deoxy-1-(3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl)-β-D-ribofuranuronamide

1-dideoxy-1-<3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl>-N-<4-(3-methylureido)phenyl>-β-D-ribofuranuronamide

1-deoxy-1-(3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl)-N-<2-(3-methylureido)ethyl>β-D-ribofuranuronamide

1-deoxy-1-(3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl)-N-<2-(3-methyl-3-nitrosoureido)ethyl>β-D-ribofuranuronamide

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