Borate(1-), tetrakis(phenylethynyl)-, ammonium

Base Information

Chemical Name:Borate(1-), tetrakis(phenylethynyl)-, ammonium
CAS No.:668983-96-8
Molecular Formula:C32H20B.H4N
Molecular Weight:433.36
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Borate(1-), tetrakis(phenylethynyl)-, ammonium

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Borate(1-), tetrakis(phenylethynyl)-, ammonium

There total 2 articles about Borate(1-), tetrakis(phenylethynyl)-, ammonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6738-06-3
phenylethynylmagnesium bromide

: 668983-96-8
tetrakis-phenylethynyl-boric acid ; ammonium salt

Guidance literature:: With potassium tetrafluoroborate;

Reference yield:

: 6738-06-3
phenylethynylmagnesium bromide

: 668983-96-8
tetrakis-phenylethynyl-boric acid ; ammonium salt

Guidance literature:

Reference yield: 73.0%

: iron(II) tris-nioximate dichloride

: 668983-96-8
tetrakis-phenylethynyl-boric acid ; ammonium salt

: 1,12-bis(phenylethynyl)-2,11,13,22,23,32-hexaoxa-3,10,14,21,24,31-hexaaza-1,12-diborapentacyclo[11.11.11.0(4,9).0(15,20).0(25,30)]ditriaconta-3,9,14,20,24,30-hexaene^(2-)iron(II)

Guidance literature:: In ethanol; (Fe(H2Nx)3)Cl2 was dissolved/suspended in EtOH, (NH4)(B(CCPh)4) was added, react. mixt. was refluxed with stirring for 5 h; ppt. was filtered off, washed with EtOH and Et2O, dissolved in CHCl3 andfiltered, heptane was added, ppt. was dried in vacuo; elem. anal.;
DOI:10.1023/A:1025641025505