2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one

Base Information

Chemical Name:2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one
CAS No.:53766-25-9
Molecular Formula:C23H24O7
Molecular Weight:412.4325
Hs Code.:
NSC Number:168806
DSSTox Substance ID:DTXSID00419370

Synonyms:53766-25-9;NSC168806;DTXSID00419370;2-(3,4-dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one

Suppliers and Price of 2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one

Chemical Property:

Vapor Pressure:2.18E-15mmHg at 25°C
Boiling Point:608.3°Cat760mmHg
Flash Point:209.7°C
Density:1.29g/cm³
XLogP3:5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:412.15220310
Heavy Atom Count:30
Complexity:667

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCOC1=CC(=C2C(=C1)OC(=C(C2=O)OC)C3=CC(=C(C=C3)OC)OC)O)C

Technology Process of 2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one

There total 3 articles about 2-(3,4-Dimethoxyphenyl)-5-hydroxy-3-methoxy-7-(3-methylbut-2-enoxy)chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 14549-84-9
quercetin 3,3',4'-trimethyl ether

: 870-63-3
prenyl bromide

: 53766-25-9
5-hydroxy-7-prenyloxy-3,3',4'-trimethoxyflavone

Guidance literature:: With potassium carbonate; In acetone; for 5h; Heating;
DOI:10.1021/jm040770b

Reference yield:

: 24824-54-2
3,4-dimethoxybenzoic anhydride

: 53766-25-9
5-hydroxy-7-prenyloxy-3,3',4'-trimethoxyflavone

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N / 0.08 h / Heating

1.2: 74 percent / KOH / methanol / 0.33 h / sonication

2.1: 74 percent / K₂CO₃ / acetone / 5 h / Heating

With potassium carbonate; triethylamine; In acetone; 1.1: Allan-Robinson condensation;
DOI:10.1021/jm040770b

Reference yield:

: 93-07-2
Veratric acid

: 53766-25-9
5-hydroxy-7-prenyloxy-3,3',4'-trimethoxyflavone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / methanesulfonyl chloride; Et₃N / tetrahydrofuran / 0 °C

2.1: Et₃N / 0.08 h / Heating

2.2: 74 percent / KOH / methanol / 0.33 h / sonication

3.1: 74 percent / K₂CO₃ / acetone / 5 h / Heating

With potassium carbonate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; acetone; 2.1: Allan-Robinson condensation;
DOI:10.1021/jm040770b