digitoxigenin-3-bromoacetate

Base Information

• Chemical Name: digitoxigenin-3-bromoacetate
• CAS No.: 31702-65-5
• Molecular Formula: C₂₅H₃₅BrO₅
• Molecular Weight: 495.454
• Mol file: 31702-65-5.mol

Synonyms:5b-Card-20(22)-enolide, 3b,14-dihydroxy-, 3-(bromoacetate)(8CI); Acetic acid, bromo-, 3-ester with 3b,14-hydroxy-5b-card-20(22)enolide; Digitoxigenin 3-bromoacetate

Chemical Property of digitoxigenin-3-bromoacetate

Chemical Property:

• Vapor Pressure: 1.27E-16mmHg at 25°C
• Boiling Point: 594.7°Cat760mmHg
• Flash Point: 313.5°C
• PSA: 72.83000
• Density: 1.38g/cm³
• LogP: 4.55010

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of digitoxigenin-3-bromoacetate

There total 2 articles about digitoxigenin-3-bromoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromoacetyl bromide (598-21-0) + (+)-digitoxigenin (143-62-4) → Digitoxigenin-3-bromacetat (31702-65-5)

Guidance literature:

DOI:10.1007/BF00714917

Reference yield:

→ Digitoxigenin-3-bromacetat (31702-65-5)

Guidance literature:

Digitoxigenin (5), Bromacetylbromid, Py. (Dioxan, 1.5h);

DOI:10.1021/jm00288a011

Reference yield:

Digitoxigenin-3-bromacetat (31702-65-5) + ajmaline → 3β-O-(ajmalin-N(b)-ioacetyl)digitoxigenin (83048-05-9)

Guidance literature:

DOI:10.1007/BF00714917

upstream raw materials:

2-Bromoacetyl bromide

(+)-digitoxigenin

Downstream raw materials:

3β-O-(ajmalin-N(b)-ioacetyl)digitoxigenin