Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide

Base Information

Chemical Name:Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide
CAS No.:670276-10-5
Molecular Formula:C13H14ClOP
Molecular Weight:252.68
Hs Code.:
DSSTox Substance ID:DTXSID40478002
Nikkaji Number:J2.032.528C,J2.112.759K

Synonyms:Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide;670276-10-5;DTXSID40478002

Suppliers and Price of Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:252.0470798
Heavy Atom Count:16
Complexity:375

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CP(=O)(C1)C2=CC=C(C=C2)C)Cl

Technology Process of Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide

There total 2 articles about Phosphorin, 4-chloro-1,2-dihydro-3-methyl-1-(4-methylphenyl)-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13829-65-7
1-(4-methylphenyl)-3-methyl-2,5-dihydro-1H-phosphole 1-oxide

: 670276-10-5
3-methyl-4-chloro-1-(4-methylphenyl)-1,2-dihydrophosphinine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / TEBAC; NaOH / H₂O / 63 °C

2: 0.12 h / 138 °C

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In water;
DOI:10.1002/hc.10176