4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide

Base Information

Chemical Name:4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide
CAS No.:75412-58-7
Molecular Formula:C₂₁H₁₇ClN₄O₄
Molecular Weight:424.843
Hs Code.:
Mol file:75412-58-7.mol

Synonyms:BRN 4597436;75412-58-7;4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide;Benzoic acid, 4-chloro-2-((2-methoxyphenyl)amino)-, ((3-nitrophenyl)methylene)hydrazide;LS-36523

Suppliers and Price of 4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide

Chemical Property:

PSA：108.54000
LogP:5.75140
XLogP3:5.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:424.0938327
Heavy Atom Count:30
Complexity:614

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1NC2=C(C=CC(=C2)Cl)C(=O)NN=CC3=CC(=CC=C3)[N+](=O)[O-]
Isomeric SMILES:COC1=CC=CC=C1NC2=C(C=CC(=C2)Cl)C(=O)N/N=C/C3=CC(=CC=C3)[N+](=O)[O-]

Technology Process of 4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide

There total 5 articles about 4-Chloro-2-((2-methoxyphenyl)amino)benzoic acid ((3-nitrophenyl)methylene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-84-0
2,4 dichlorobenzoic acid

: 75412-58-7
4-Chloro-2-(2-methoxy-phenylamino)-benzoic acid [1-(3-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃, copper powder / pentan-1-ol

2: SOCl₂ / 12 h / Heating

3: hydrazine hydrate / ethanol / 16 h / Heating

4: gl. acetic acid / ethanol / 4 h / Heating

With thionyl chloride; copper; potassium carbonate; hydrazine hydrate; acetic acid; In ethanol; pentan-1-ol;

Reference yield:

: 32305-23-0
N-(2-Methoxyphenyl)-4-chloroanthranilic acid

: 75412-58-7
4-Chloro-2-(2-methoxy-phenylamino)-benzoic acid [1-(3-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 12 h / Heating

2: hydrazine hydrate / ethanol / 16 h / Heating

3: gl. acetic acid / ethanol / 4 h / Heating

With thionyl chloride; hydrazine hydrate; acetic acid; In ethanol;

Reference yield:

: 23857-11-6
4-chloro-2-(2-methoxy-anilino)-benzoic acid methyl ester

: 75412-58-7
4-Chloro-2-(2-methoxy-phenylamino)-benzoic acid [1-(3-nitro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 16 h / Heating

2: gl. acetic acid / ethanol / 4 h / Heating

With hydrazine hydrate; acetic acid; In ethanol;