1,3,5-Trioxa-2,4-disila-6-boracyclohexane, 2,2,4,4-tetramethyl-6-phenyl-

Base Information

Chemical Name:1,3,5-Trioxa-2,4-disila-6-boracyclohexane, 2,2,4,4-tetramethyl-6-phenyl-
CAS No.:67133-55-5
Molecular Formula:C10H17BO3Si2
Molecular Weight:252.225
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,5-Trioxa-2,4-disila-6-boracyclohexane, 2,2,4,4-tetramethyl-6-phenyl-

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,3,5-Trioxa-2,4-disila-6-boracyclohexane, 2,2,4,4-tetramethyl-6-phenyl-

There total 7 articles about 1,3,5-Trioxa-2,4-disila-6-boracyclohexane, 2,2,4,4-tetramethyl-6-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 2401-73-2
1,1,3,3-tetramethyl-1,3-dichlorodisiloxane

: 98-80-6
phenylboronic acid

: 141613-69-6
(C₆H₅BO)((CH₃)2SiO)4

: 141613-70-9
(C₆H₅BO)2((CH₃)2SiO)4

: 67133-55-5
2,2,4,4-Tetramethyl-6-phenyl-[1,3,5,2,4,6]trioxadisilaborinane

Guidance literature:: With N(C₂H₅)3; In not given; byproducts: {N(C2H5)3H}Cl; (3+3) cyclocondensation reaction of 1,3-dichlorotetramethyldisiloxane with phenylboric acid in the presence of triethylamine as a hydrogen halide acceptor;; product mixture obtained; detected by (29)Si NMR; (C6H5BO)((CH3)2SiO)2 was purified by vacuum distillation;;

Reference yield: 30.0%

: 3277-26-7
1,1,3,3-Tetramethyldisiloxane

: 98-80-6
phenylboronic acid

: 67133-55-5
2,2,4,4-Tetramethyl-6-phenyl-[1,3,5,2,4,6]trioxadisilaborinane

Guidance literature:: With tris(pentafluorophenyl)borate; In benzene; at 25 ℃; for 4h;

Reference yield: 10.0%

: 141613-68-5
(C₆H₅BO)((CH₃)2SiO)3

: 141613-69-6
(C₆H₅BO)((CH₃)2SiO)4

: 67133-55-5
2,2,4,4-Tetramethyl-6-phenyl-[1,3,5,2,4,6]trioxadisilaborinane

Guidance literature:: In melt; byproducts: {PhBO}3, {Me2SiO}3, {Me2SiO}4; heating at 225 °C in an evacuated sealed Pyrex tube for 4 h; further byproducts obtained;; residue dissolved in dry Et2O, the resulting soln. was filtered to remove (PhBO)3, the solvent was then removed carefully under low vacuum (100mmHg); residue dissolved in C6D6 and analyzed by (29)Si NMR spectroscopy;product mixture; not isolated;;