Octadecanedioic acid, 9-hydroxy-10-oxo-, dimethyl ester

Base Information

Chemical Name:Octadecanedioic acid, 9-hydroxy-10-oxo-, dimethyl ester
CAS No.:67136-05-4
Molecular Formula:C20H36O6
Molecular Weight:372.502
Hs Code.:

Synonyms:

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Chemical Property of Octadecanedioic acid, 9-hydroxy-10-oxo-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Octadecanedioic acid, 9-hydroxy-10-oxo-, dimethyl ester

There total 8 articles about Octadecanedioic acid, 9-hydroxy-10-oxo-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7297-29-2
methyl 9⁽¹⁰⁾-hydroxy 10⁽⁹⁾-oxo octadecanoate

: 124-19-6
nonan-1-al

: 4444-91-1
methyl 9-hydroxy-10-oxostearate

: 1931-63-1
methyl ester of azelaic acid aldehyde

: 67136-05-4
dimethyl 9-hydroxy-10-oxooctadecanedioate

Guidance literature:: With N-methyl-4,5-dimethylthiazolium iodide; potassium carbonate; In acetonitrile; at 170 ℃; for 1h; Reagent/catalyst; Temperature; Microwave irradiation; Inert atmosphere;
DOI:10.1002/cssc.201500462

Reference yield:

: 112-62-9
Methyl oleate

: 124-19-6
nonan-1-al

: 4444-91-1
methyl 9-hydroxy-10-oxostearate

: 1931-63-1
methyl ester of azelaic acid aldehyde

: 67136-05-4
dimethyl 9-hydroxy-10-oxooctadecanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid; dihydrogen peroxide / neat (no solvent) / 8 h / 20 - 30 °C / Cooling with ice

2: boron trifluoride diethyl etherate / dimethyl sulfoxide / 22 h / 80 °C / Inert atmosphere

3: N-methyl-4,5-dimethylthiazolium iodide; potassium carbonate / acetonitrile / 1 h / 170 °C / Microwave irradiation; Inert atmosphere

With formic acid; boron trifluoride diethyl etherate; dihydrogen peroxide; N-methyl-4,5-dimethylthiazolium iodide; potassium carbonate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1002/cssc.201500462

Reference yield:

: 2566-91-8
epoxidized methyl oleate

: 124-19-6
nonan-1-al

: 4444-91-1
methyl 9-hydroxy-10-oxostearate

: 1931-63-1
methyl ester of azelaic acid aldehyde

: 67136-05-4
dimethyl 9-hydroxy-10-oxooctadecanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dimethyl sulfoxide / 22 h / 80 °C / Inert atmosphere

2: N-methyl-4,5-dimethylthiazolium iodide; potassium carbonate / acetonitrile / 1 h / 170 °C / Microwave irradiation; Inert atmosphere

With boron trifluoride diethyl etherate; N-methyl-4,5-dimethylthiazolium iodide; potassium carbonate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1002/cssc.201500462