5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Base Information

Chemical Name:5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one
CAS No.:67159-85-7
Molecular Formula:C11H11BrO
Molecular Weight:239.10800
Hs Code.:
DSSTox Substance ID:DTXSID501241664
Nikkaji Number:J3.452.563C

Synonyms:67159-85-7;5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one;5-Bromo-3,3-dimethyl-1-indanone;5-bromo-2,3-dihydro-3,3-dimethylinden-1-one;1H-Inden-1-one, 5-bromo-2,3-dihydro-3,3-dimethyl-;5-bromo-3,3-dimethyl-2H-inden-1-one;MFCD27927273;5-Bromo-3,3-dimethyl-indan-1-one;SCHEMBL3361527;MVIGYOCYIUJCGE-UHFFFAOYSA-N;DTXSID501241664;AKOS027339826;AS-65678;SY046165;CS-0147252;F12557;A902143;5-Bromo-2,3-dihydro-3,3-dimethyl-1H-inden-1-one

Suppliers and Price of 5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one 95%
5g
$ 1417.00

Ambeed
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one 95%
250mg
$ 174.00

Ambeed
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one 95%
100mg
$ 127.00

Ambeed
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one 95%
1g
$ 434.00

Alichem
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one
100mg
$ 185.00

Alichem
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one
1g
$ 740.00

AK Scientific
5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one
1g
$ 645.00

Total 6 raw suppliers

Chemical Property of 5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Chemical Property:

Melting Point:104 - 110 °C
Boiling Point:314.5±41.0 °C(Predicted)
PSA：17.07000
Density:1.409±0.06 g/cm3(Predicted)
LogP:3.31310
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:237.99933
Heavy Atom Count:13
Complexity:234

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CC(=O)C2=C1C=C(C=C2)Br)C

Technology Process of 5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

There total 7 articles about 5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 67159-88-0
6-bromo-2,3-dihydro-1,1-dimethyl-1H-indene

: 67159-85-7
5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Guidance literature:: 6-bromo-2,3-dihydro-1,1-dimethyl-1H-indene; With magnesium sulfate; In water; acetone;

With potassium permanganate; In water; acetone; for 5h; Reflux;

Reference yield: 75.0%

: 67159-85-7
5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Guidance literature:

Reference yield: 71.0%

: 3-(3-bromophenyl)-3-methylcyclobutanone

: 67159-85-7
5-bromo-3,3-dimethyl-2,3-dihydro-1H-inden-1-one

Guidance literature:: 3-(3-bromophenyl)-3-methylcyclobutanone; With 2-aminopyridine; Wilkinson's catalyst; benzoic acid; In para-xylene; at 150 ℃; for 20h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In water; at 20 ℃; for 1.5h; Reagent/catalyst;
DOI:10.1039/c5cc01415h