(3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)

Base Information

Chemical Name:(3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)
CAS No.:67675-20-1
Molecular Formula:C₃₂H₄₃NO
Molecular Weight:457.7
Hs Code.:

(3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)

Synonyms:

Suppliers and Price of (3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)

Chemical Property:

Vapor Pressure:5.79E-16mmHg at 25°C
Boiling Point:614.6°Cat760mmHg
Flash Point:52°C
Density:1.11g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name)

There total 3 articles about (3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(2S)-1-(naphthalen-2-ylamino)propan-2-yl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 67675-22-3
Acetic acid (3S,8S,9S,10R,13S,14S,17R)-10,13-dimethyl-17-[(S)-1-(naphthalen-2-ylcarbamoyl)-ethyl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 67675-20-1
22-(2'-naphthylamino)-23,24-dinorchol-5-en-3β-ol

: (S)-2-((3S,8S,9S,10R,13S,14S,17R)-3-Hydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-N-naphthalen-2-yl-propionamide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 72h; Yields of byproduct given; Heating;

Reference yield:

: 1474-14-2
3β-acetoxybisnor-5-cholenic acid

: 67675-20-1
22-(2'-naphthylamino)-23,24-dinorchol-5-en-3β-ol

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / dimethylformamide / 1.5 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / Ambient temperature

3: 57 percent / LiAlH₄ / tetrahydrofuran / 72 h / Heating

With lithium aluminium tetrahydride; oxalyl dichloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 67711-02-8,55103-88-3
3β-acetoxy-23,24-dinorchol-5-en-22-oyl chloride

: 67675-20-1
22-(2'-naphthylamino)-23,24-dinorchol-5-en-3β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: 57 percent / LiAlH₄ / tetrahydrofuran / 72 h / Heating

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;