3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile

Base Information

Chemical Name:3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile
CAS No.:67171-82-8
Molecular Formula:C18H33N3O
Molecular Weight:307.47400
Hs Code.:
Mol file:67171-82-8.mol

Synonyms:N-(6-Cyano-4-azahexyl)-12-dodecanlactam;13-(6-Cyan-4-aza-hexyl)-12-dodecanlactam;

Suppliers and Price of 3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile

Chemical Property:

Melting Point:39-40 °C
Boiling Point:513.4±35.0 °C(Predicted)
PKA:8.21±0.19(Predicted)
PSA：56.13000
Density:0.949±0.06 g/cm3(Predicted)
LogP:3.95178

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile

There total 1 articles about 3-[[3-(2-Oxoazacyclotridecan-1-yl)propyl]amino]propanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67171-82-8
7-(2-oxo-azacyclotridec-1-yl)-4-azaheptanenitrile

Guidance literature:: 13-(3-Amino-propyl)-12-dodecanlactam (6), Acrylonitril;
DOI:10.1002/hlca.19780610417

Reference yield: 75.0%

: 67171-82-8
7-(2-oxo-azacyclotridec-1-yl)-4-azaheptanenitrile

: 67171-89-5
3-(6-oxo-1,5-diazacycloheptadec-5-yl)propionitrile

Guidance literature:: With 1,2-Dimethyl-1,2-dihydropyridin; for 5h; Heating;
DOI:10.1002/hlca.19850680325

Reference yield:

: 67171-82-8
7-(2-oxo-azacyclotridec-1-yl)-4-azaheptanenitrile

: 64414-58-0
13-Aza-16-hexadecanlactam

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1,2-dimethylpyridine / 5 h / Heating

2: 92 percent / t-BuOK / toluene / 0.08 h / Heating

With 1,2-Dimethyl-1,2-dihydropyridin; potassium tert-butylate; In toluene;
DOI:10.1002/hlca.19850680325